Micromachined chemical sensor with integrated microelectronics

Conference · Wed Jan 01 04:00:00 EST 1992

OSTI ID:6474557

Smith, J; Sniegowski, J; Koehler, D; Ricco, T; Martin, S; McWhorter, P

With today's continued emphasis on environmental safety and health issues, a resurgence of interest has developed in the area of chemical sensors. These sensors would typically be used to monitor contamination hazards such as underground storage tanks or to assess previous contamination at waste disposal sites. Human exposure to chemical hazards can also be monitored. Additionally, these sensors can be used as part of a manufacturing process control loop. One type of sensor suitable for gas phase monitoring of chemicals is the quartz resonator or quartz crystal microbalance (QCM) sensor. In this type of sensor, a thickness shear mode (TSM) quartz resonator is coated with a film that interacts with the chemical species of interest. Changes in the mass and elasticity of this film are reflected as changes in the resonant properties of the device. Therefore, the presence of the species of interest can be detected by monitoring the frequency of an oscillator based on the resonance of the quartz. These QCM sensors compete with surface acoustic wave (SAW) devices as a means for monitoring gas phase species. SAW devices are typically more sensitive to small amounts of a species, but the instrumentation associated with a SAW device is an order of magnitude more expensive than the instrumentation associated with a TSM wave resonator since the SAW devices operate in the 100's of MHz frequency regime while quartz resonators operate in the 5--25 MHz regime. We are working to improve the sensitivity of the QCM sensor by increasing the frequency of the device to 25 MHz (compared to the typical 5 MHz crystal) and by increasing the frequency stability of the system to an ultimate goal of 0.1 Hz. The 25 MHz QCM has already been achieved and once the stability goal is achieved, the QCM will have the same sensitivity as a SAW device.

• Research Organization: Sandia National Labs., Albuquerque, NM (United States)
• Sponsoring Organization: DOE; USDOE, Washington, DC (United States)
• DOE Contract Number: AC04-76DP00789
• OSTI ID: 6474557
• Report Number(s): SAND-92-2623C; CONF-9305110--1; ON: DE93013761
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400102 -- Chemical & Spectral Procedures
440800* -- Miscellaneous Instrumentation-- (1990-)
47 OTHER INSTRUMENTATION
DESIGN
DETECTION
ELECTRONIC CIRCUITS
ELECTRONIC EQUIPMENT
EQUIPMENT
FILMS
GAS ANALYSIS
INTEGRATED CIRCUITS
MICROELECTRONIC CIRCUITS
MICROELECTRONICS
MINERALS
ORGANIC COMPOUNDS
OSCILLATORS
OXIDE MINERALS
PHYSICAL PROPERTIES
QUARTZ
RESONATORS
THERMODYNAMIC PROPERTIES
THIN FILMS