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Determination of traces of arsenic: a review

Conference · · ACS Symp. Ser.; (United States)
OSTI ID:6391872
This review was organized in terms of the main steps and topics characterizing all trace analysis: sample pretreatment and dissolution, solution stability, preconcentration, isolation and determination. Pretreatment methods included wet ashing, dry ashing, oxygen combustion, and fusion. Methods used for preconcentration included: coprecipitation and adsorption, liquid-liquid extraction, and volatilization. The methods used for determination were: (1) molecular absorption-spectrophotometry; (2) radiochemical techniques; (3) electrochemical techniques such as amperometric titrations, polarography, and coulometry; (4) x-ray fluorescence spectroscopy; and (5) atomic spectroscopy including atomic emission spectroscopy, atomic absorption spectrometry, and chromatographic methods. 161 references, 5 figures.
Research Organization:
Oak Ridge National Lab., TN
DOE Contract Number:
W-7405-ENG-26
OSTI ID:
6391872
Conference Information:
Journal Name: ACS Symp. Ser.; (United States) Journal Volume: 7:21
Country of Publication:
United States
Language:
English