Identification and toxicity of fractionated-shale-oil components
Technical Report
·
OSTI ID:6379616
A procedure for the separation and identification of polynuclear aromatic hydrocarbons (PNAs) in shale oil is presented. This procedure comprises two steps. First, the shale oil is separated into fractions according to ring size on a Chromosorb LC-9 normal phase column. Then each of these fractions are separated into individual components and identified using an analytical reversed-phase Ultrasphere ODS 5..mu..m column. In addition, toxicity studies are carried out on each fraction obtained from the amine column to indicate which class of PNAs warrants special attention and analysis. The results of this approach are reported here.
- Research Organization:
- Texas A and M Univ., College Station (USA)
- DOE Contract Number:
- AS05-80EV10404
- OSTI ID:
- 6379616
- Report Number(s):
- DOE/EV/10404-T1; ON: DE81028460
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
04 OIL SHALES AND TAR SANDS
040500* -- Oil Shales & Tar Sands-- Properties & Composition
040700 -- Oil Shales & Tar Sands-- Health & Safety
560301 -- Chemicals Metabolism & Toxicology-- Cells-- (-1987)
63 RADIATION, THERMAL, AND OTHER ENVIRON. POLLUTANT EFFECTS ON LIVING ORGS. AND BIOL. MAT.
ANIMALS
ANTHRACENE
AROMATICS
CELL CULTURES
CHEMICAL ANALYSIS
CHROMATOGRAPHY
CONDENSED AROMATICS
ENERGY SOURCES
FLUORENE
FOSSIL FUELS
FRACTIONATION
FUELS
HAMSTERS
HYDROCARBONS
LIQUID COLUMN CHROMATOGRAPHY
MAMMALS
MINERAL OILS
OILS
ORGANIC COMPOUNDS
OTHER ORGANIC COMPOUNDS
PHENANTHRENE
POLYCYCLIC AROMATIC HYDROCARBONS
RODENTS
SEPARATION PROCESSES
SHALE OIL
TOXICITY
VERTEBRATES
040500* -- Oil Shales & Tar Sands-- Properties & Composition
040700 -- Oil Shales & Tar Sands-- Health & Safety
560301 -- Chemicals Metabolism & Toxicology-- Cells-- (-1987)
63 RADIATION, THERMAL, AND OTHER ENVIRON. POLLUTANT EFFECTS ON LIVING ORGS. AND BIOL. MAT.
ANIMALS
ANTHRACENE
AROMATICS
CELL CULTURES
CHEMICAL ANALYSIS
CHROMATOGRAPHY
CONDENSED AROMATICS
ENERGY SOURCES
FLUORENE
FOSSIL FUELS
FRACTIONATION
FUELS
HAMSTERS
HYDROCARBONS
LIQUID COLUMN CHROMATOGRAPHY
MAMMALS
MINERAL OILS
OILS
ORGANIC COMPOUNDS
OTHER ORGANIC COMPOUNDS
PHENANTHRENE
POLYCYCLIC AROMATIC HYDROCARBONS
RODENTS
SEPARATION PROCESSES
SHALE OIL
TOXICITY
VERTEBRATES