Method of purifying uranium tetrafluoride hydrate and preparing uranium (VI) peroxide hydrate using a fluoride precipitating agent
Patent
·
OSTI ID:6364693
A method is described for preparing uranium (VI) peroxide hydrate from uranium tetrafluoride hydrate, comprising the steps of digesting uranium tetrafluoride hydrate in an aqueous acid in the presence of a fluoride precipitating agent to produce an aqueous uranium solution, filtering the aqueous uranium solution to remove precipitated fluorides and undissolved material, adjusting the aqueous uranium solution to a ph between about 1 to about 3, reacting the aqueous uranium solution with peroxide to precipitate uranium (VI) peroxide hydrate, and separating the precipitated uranium (VI) peroxide hydrate.
- Assignee:
- Gardinier Inc
- Patent Number(s):
- US 4247522
- OSTI ID:
- 6364693
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
050400* -- Nuclear Fuels-- Feed Processing
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS
ACTINIDE COMPOUNDS
CHEMICAL PREPARATION
DIGESTION
FILTRATION
FLUORIDES
FLUORINE COMPOUNDS
HALIDES
HALOGEN COMPOUNDS
HYDRATES
HYDROGEN COMPOUNDS
INORGANIC ACIDS
NITRIC ACID
OXYGEN COMPOUNDS
PEROXIDES
PRECIPITATION
PURIFICATION
SEPARATION PROCESSES
SYNTHESIS
URANIUM COMPOUNDS
URANIUM FLUORIDES
URANIUM PEROXIDES
URANIUM TETRAFLUORIDE
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS
ACTINIDE COMPOUNDS
CHEMICAL PREPARATION
DIGESTION
FILTRATION
FLUORIDES
FLUORINE COMPOUNDS
HALIDES
HALOGEN COMPOUNDS
HYDRATES
HYDROGEN COMPOUNDS
INORGANIC ACIDS
NITRIC ACID
OXYGEN COMPOUNDS
PEROXIDES
PRECIPITATION
PURIFICATION
SEPARATION PROCESSES
SYNTHESIS
URANIUM COMPOUNDS
URANIUM FLUORIDES
URANIUM PEROXIDES
URANIUM TETRAFLUORIDE