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Test results of a diamond double-crystal monochromator at the advanced photon source

Journal Article · · AIP Conference Proceedings
DOI:https://doi.org/10.1063/1.54594· OSTI ID:627872
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  1. Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois60439 (United States)

We have tested the first diamond double-crystal monochromator at the Advanced Photon Source (APS). The monochromator consisted of two synthetic type 1b (111) diamond plates in symmetric Bragg geometry. We tested two pairs of single-crystal plates: the first pair was 6 mm by 5 mm by 0.25 mm and 6 mm by 5 mm by 0.37 mm; the second set was 7 mm by 5.5 mm by 0.44 mm. The monochromator first crystal was indirectly cooled by edge contact with a water-cooled copper holder. We studied the performance of the monochromator under the high-power x-ray beam delivered by the APS undulator A. We found no indication of thermal distortions or strains even at the highest incident power (280 watts) and power density (123W/mm{sup 2} at normal incidence). The calculated maximum power and power density absorbed by the first crystal were 37 watts and 4.3W/mm{sup 2}, respectively. We also compared the maximum intensity delivered by the diamond monochromator and by a silicon (111) cryogenically cooled monochromator. For energies in the range of 6 to 10 keV, the flux through the diamond monochromator was about a factor of two less than through the silicon monochromator, in good agreement with calculations. We conclude that water-cooled diamond monochromators can handle the high-power beams from the undulator beamlines at the APS. As single-crystal diamond plates of larger size and better quality become available, the use of diamond monochromators will become a very attractive option. {copyright} {ital 1997 American Institute of Physics.}

Research Organization:
Argonne National Laboratory (ANL), Argonne, IL
Sponsoring Organization:
USDOE
DOE Contract Number:
W-31109-ENG-38
OSTI ID:
627872
Report Number(s):
CONF-9706157--
Journal Information:
AIP Conference Proceedings, Journal Name: AIP Conference Proceedings Journal Issue: 1 Vol. 417; ISSN APCPCS; ISSN 0094-243X
Country of Publication:
United States
Language:
English

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