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Title: Test results of a diamond double-crystal monochromator at the advanced photon source

Conference ·
OSTI ID:555247

We have tested the first diamond double-crystal monochromator at the Advanced Photon Source (APS). The monochromator consisted of two synthetic type lb (111) diamond plates in symmetric Bragg geometry. We tested two pairs of single-crystal plates: the first pair was 6 mm by 5 mm by 0.25 mm and 6 mm by 5 mm by 0.37 mm; the second set was 7 mm by 5.5 mm by 0.44 mm. The monochromator first crystal was indirectly cooled by edge contact with a water-cooled copper holder. We studied the performance of the monochromator under the high-power x-ray beam delivered by the APS undulator A. We found no indication of thermal distortions or strains even at the highest incident power (280 watts) and power density (123 W/mm{sup 2} at normal incidence). The calculated maximum power and power density absorbed by the first crystal were 37 watts and 16 W/mm{sup 2} respectively. We also compared the maximum intensity delivered by the diamond monochromator and by a silicon (111) cryogenically cooled monochromator. For energies in the range of 6 to 10 keV, the flux through the diamond monochromator was about a factor of two less than through the silicon monochromator, in good agreement with calculations. We conclude that water-cooled diamond monochromators can handle the high-power beams from the undulator beams from the undulator beamlines at the APS. As single-crystal diamond plates of larger size and better quality become available, the use of diamond monochromators will become a very attractive option.

Research Organization:
Argonne National Lab. (ANL), Argonne, IL (United States)
Sponsoring Organization:
USDOE Office of Energy Research, Washington, DC (United States)
DOE Contract Number:
W-31-109-ENG-38
OSTI ID:
555247
Report Number(s):
ANL/XFD/CP-93477; CONF-9706157-; ON: DE97053649; TRN: 98:008601
Resource Relation:
Conference: SRI `97: 10. U.S. national conference on synchrotron radiation instrumentation, Ithaca, NY (United States), 17-20 Jun 1997; Other Information: PBD: Jun 1997
Country of Publication:
United States
Language:
English