An x-ray microprobe facility using synchrotron radiation
A x-ray microprobe for trace elemental analysis at micrometer spatial resolutions using synchrotron radiation (SR) is under development. The facility consists of two beamlines, one including a 1:1 focusing mirror and the other an 8:1 ellipsoidal mirror. At present ''white light''' is used for excitation of the characteristic x-ray fluorescence lines. Sensitivities in thin biological samples are in the range of 2-20 fg in 100 ..mu..m/sup 2/ areas in 5 min irradiation times. Scanning techniques as well as microtomography and chemical speciation are discussed. Application to a specific biomedical study is included. 13 refs., 2 figs.
- Research Organization:
- Brookhaven National Lab., Upton, NY (USA)
- DOE Contract Number:
- AC02-76CH00016
- OSTI ID:
- 6263258
- Report Number(s):
- BNL-42711; CONF-890410-2; ON: DE89012973
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400101* -- Activation
Nuclear Reaction
Radiometric & Radiochemical Procedures
43 PARTICLE ACCELERATORS
430400 -- Particle Accelerators-- Storage Rings
550000 -- Biomedical Sciences
Basic Studies
59 BASIC BIOLOGICAL SCIENCES
ACCELERATORS
BIOLOGICAL MATERIALS
BREMSSTRAHLUNG
CHEMICAL ANALYSIS
CYCLIC ACCELERATORS
DIAGNOSTIC TECHNIQUES
ELECTROMAGNETIC RADIATION
MATERIALS
MICROANALYSIS
NONDESTRUCTIVE ANALYSIS
NSLS
RADIATION SOURCES
RADIATIONS
SYNCHROTRON RADIATION
SYNCHROTRON RADIATION SOURCES
SYNCHROTRONS
TOMOGRAPHY
TRACE AMOUNTS
X-RAY EMISSION ANALYSIS
X-RAY FLUORESCENCE ANALYSIS
400101* -- Activation
Nuclear Reaction
Radiometric & Radiochemical Procedures
43 PARTICLE ACCELERATORS
430400 -- Particle Accelerators-- Storage Rings
550000 -- Biomedical Sciences
Basic Studies
59 BASIC BIOLOGICAL SCIENCES
ACCELERATORS
BIOLOGICAL MATERIALS
BREMSSTRAHLUNG
CHEMICAL ANALYSIS
CYCLIC ACCELERATORS
DIAGNOSTIC TECHNIQUES
ELECTROMAGNETIC RADIATION
MATERIALS
MICROANALYSIS
NONDESTRUCTIVE ANALYSIS
NSLS
RADIATION SOURCES
RADIATIONS
SYNCHROTRON RADIATION
SYNCHROTRON RADIATION SOURCES
SYNCHROTRONS
TOMOGRAPHY
TRACE AMOUNTS
X-RAY EMISSION ANALYSIS
X-RAY FLUORESCENCE ANALYSIS