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Tris(phenyl(difluorophosphino)amino)phosphine (P(N(C/sub 6/H/sub 5/)PF/sub 2/)/sub 3/), a novel tridentate strong. pi. -acceptor ligand forming cage chelates. Crystal structure of the chelate complex P(N(C/sub 6/H/sub 5/)PF/sub 2/)/sub 3/MO(CO)/sub 3/

Journal Article · · J. Am. Chem. Soc.; (United States)
DOI:https://doi.org/10.1021/ja00407a056· OSTI ID:6243823

The space group of P(N(C/sub 6/H/sub 5/)PF/sub 2/)/sub 3/ Mo(CO)/sub 3/ is P2/sub 1//c. The unit cell parameters are a = 8.683(1) A, b = 28.218(7) A, c = 15.338 (2) A, and ..beta.. = 118.12 (1)/sup 0/. The structure is that of an octahedral fac-L/sub 3/ Mo(CO)/sub 3/ complex. The ligand has its PF/sub 2/ groups linked to the Mo atom. (DLC)

DOE Contract Number:
W-7405-ENG-26
OSTI ID:
6243823
Journal Information:
J. Am. Chem. Soc.; (United States), Journal Name: J. Am. Chem. Soc.; (United States) Vol. 103:17; ISSN JACSA
Country of Publication:
United States
Language:
English