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Liquefaction of lignite by the COSTEAM process

Technical Report ·
OSTI ID:6161838
Carbon monoxide, 0.7 H/sub 2/:1.0 CO and 3 H/sub 2/:1 CO mole ratio synthesis gases were employed in a process variable study of the parameters influencing the oil yield from a North Dakota lignite. A slurry composed of 30 wt % pulverized coal in anthracene oil was pumped in continuous operations into a one-liter stirred reactor where effective interphase contact was achieved by a turbine type agitator. Pressures of 2000, 3000, and 4000 psig; temperatures from 375 to 450/sup 0/C and residence times of 1 and 2 hours were among the parameters evaluated. Oil yields of greater than 60 wt % of the moisture and ash free (m.a.f.) lignite were attained with carbon monoxide and 3 H/sub 2/:1 CO synthesis gas at 4000 psig, 400 and 425/sup 0/C respectively, and 2 hours residence time; a maximum oil yield of 52 wt % was attained with 0.7 H/sub 2/:1 CO process gas. 6 figures, 3 tables.
Research Organization:
Department of Energy, Pittsburgh, PA (USA). Pittsburgh Energy Research Center
OSTI ID:
6161838
Report Number(s):
CONF-750329-5; ON: DE83008208
Country of Publication:
United States
Language:
English

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