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Title: Calibration of an argon in germanium standard using Rutherford backscattering spectrometry for energy dispersive x-ray spectroscopy

Journal Article · · J. Vac. Sci. Technol., A; (United States)
DOI:https://doi.org/10.1116/1.576180· OSTI ID:6056842

An argon standard for energy dispersive x-ray spectroscopy (EDS) has been made by bias sputtering hydrogenated amorphous germanium (/ital a/-Ge:H) films and determining the concentration of argon with Rutherford backscattering spectrometry. Varying concentrations of argon in hydrogenated amorphous germanium were achieved by changing the dc bias on the substrate holder and the gas pressure during rf magnetron sputtering onto a silicon substrate. It was found that standardless EDS analysis underestimates the argon concentration by about a factor of 2.

Research Organization:
Department of Nuclear Engineering, Phoenix Memorial Laboratory, The University of Michigan, Ann Arbor, Michigan 48109-2100(US); Energy Conversion Devices, Inc., Troy, Michigan 48084; Department of Nuclear Engineering, Phoenix Memorial Laboratory, The University of Michigan, Ann Arbor, Michigan 48109-2100
OSTI ID:
6056842
Journal Information:
J. Vac. Sci. Technol., A; (United States), Vol. 7:4
Country of Publication:
United States
Language:
English