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U.S. Department of Energy
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Elastic behavior of single crystals of yttria-stabilized zirconia

Thesis/Dissertation ·
OSTI ID:6019272

The single-crystalline elastic constants of yttria-stabilized zirconia (YSZ) were determined over the temperature range 20 to 700/sup 0/C by the pulse-echo-overlap technique. Different crystals of YSZ containing 8.1, 11.1, 12.1, 15.5, and 17.9 mol % Y/sub 2/O/sub 3/ were examined. The compositional dependencies of the three independent constants at room temperature show that, upon increasing Y/sub 2/O/sub 3/ content, C/sub 11/ decreases, whereas C/sub 12/ and C/sub 44/ increase. All conventional constants show normal negative temperature dependencies except those of the 8.1 mol % Y/sub 2/O/sub 3/ alloy, which show nonreproducible behaviors at elevated temperatures. Shear anisotropy in YSZ is pronounced and it decreases with increasing Y/sub 2/O/sub 3/ content but increases with temperature. Extrapolation of longitudinal and shear constants along different crystallographic directions at room temperature indicates elastic isotropy near 40 mol % Y/sub 2/O/sub 3/ where a number of investigations have established the presence of an ordered phase (Zr/sub 3/Y/sub 4/O/sub 12/) with a rhombohedral symmetry.

OSTI ID:
6019272
Country of Publication:
United States
Language:
English