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Title: Cryostat with external refrigerator for super-conducting NMR spectrometer

Patent ·
OSTI ID:5806113

An improved cryostat for the superconducting magnet of an NMR spectrometer comprises a nested structure of isothermal shells surrounding a thermally conductive central reservoir of substantially spherical shape containing liquid helium in which the superconducting solenoid remains operational when only partially immersed. A radiation shield surrounding the central reservoir is cooled by the boil-off of escaping helium vapor. The radiation shield is enclosed within a isothermal shell maintained at the temperature of liquid nitrogen by thermal contact with a liquid nitrogen reservoir disposed above the region of the central reservoir and shielded therefrom by a wall of the isothermal shell. An outer radiation shield surrounds the liquid nitrogen reservoir and associated isothermal shell and the outer radiation shield is maintained at a temperatures of the order of 180* K. By an external refrigeration facility. A hermitica sealed containment vessel forms the outer wall of the cryostat and provides a port for evacuating to a very low common pressure all the interior spaces between adjacent nested structures. The spacing between adjacent nested surfaces is maintained by a novel internal mechanical bracing system of low thermal conductivity comprising polyester cords disposed under tension between adjacent shells.

Assignee:
Varian Associates Inc
Patent Number(s):
US 4291541
Application Number:
TRN: 82-005037
OSTI ID:
5806113
Resource Relation:
Patent File Date: Filed date 30 Jun 1980
Country of Publication:
United States
Language:
English