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Preparation of the textured Bi-based oxide tapes by partial melting process

Conference · · IEEE Transactions on Magnetics (Institute of Electrical and Electronics Engineers); (United States)
OSTI ID:5767324
;  [1]; ; ; ;  [2]
  1. Asahi Glass Co. Ltd., Yokohama (Japan). Research Lab.
  2. National Research Inst. for Metals, Tsukuba, Ibaraki (Japan). Tsukuba Lab.
This paper reports on Bi{sub 2}Sr{sub 2}Ca{sub 1}Cu{sub 2}O{sub x} textured tapes with an excellent J{sub c} prepared by doctor-blade casting and a partial melt process. A green tape, composed of Bi{sub 2}Sr{sub 2}Cu{sub 1}O{sub x} powder and organic formulation was laid on a silver foil and heat treated. A highly textured microstructure was formed during slow cooling between 890{degrees}C and 870{degrees}C. XRD and SEM observation indicated that initially an oriented Bi{sub 2}Sr{sub 2}Cu{sub 2}O{sub x} structure forms by growth from the melt and it subsequently transforms to the Bi{sub 2}Sr{sub 2}Ca{sub 1}Cu{sub 2}O{sub x} phase. A grain alignment was significantly enhanced in oxide layer with a thickness less than 20{mu}m. Silver dissolved in the oxide from substrate also plays an important role for the grain alignment by lowering the melting point of the oxide.
OSTI ID:
5767324
Report Number(s):
CONF-900944--
Conference Information:
Journal Name: IEEE Transactions on Magnetics (Institute of Electrical and Electronics Engineers); (United States) Journal Volume: 27:2
Country of Publication:
United States
Language:
English