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U.S. Department of Energy
Office of Scientific and Technical Information

Investigation of vaporization and devolatilization of coal/water mixtures. Fifth quarterly report, May 1, 1983-July 31, 1983

Technical Report ·
OSTI ID:5542969

The objective of this program is to develop the capabilities to predict the vaporization and devolatilization behavior of coal/water mixtures under conditions appropriate for spray combustion. The program is currently collecting data in an entrained flow coal reactor which has a fixed position, coal/water slurry spray injector and a movable product extractor. This reactor is being used to study the vaporization and pyrolysis of coal/water slurries. FT-IR is used for the analysis of the product gases, tars and chars to determine species evolution kinetics and kinetics of secondary reactions such as steam-char reactions, cracking, soot formation, char gasification, cenophere formation and particle swelling, and char reactivity. Temperature measurements were made along the center line of the test section of the reactor by removing the collection system and inserting a suction pyrometer through the bottom of the reactor. The temperature profile is quite constant in the top 40 cm of the reactor, but then drops off about 150/sup 0/ in the lower 20 cm. Data for the Pittsburgh Seam coal/water slurry were collected at furnace temperatures of 1100/sup 0/C and 1300/sup 0/C. The general behavior of the various species indicates more conversion of aliphatic to CO and CO/sub 2/, compared to dry coal pyrolysis. Chars from slurry pyrolyses at 1100/sup 0/C and 1300/sup 0/C show substantial agglomeration, with the 1300/sup 0/C char showing the largest effect. The char particles from the water coinjection case appear to be individual coal particles which have swelled into cenospheres, whereas with the slurry there are clearly many coal particles.

Research Organization:
Advanced Fuel Research, Inc., East Hartford, CT (USA)
DOE Contract Number:
AC22-82PC50254
OSTI ID:
5542969
Report Number(s):
DOE/PC/50254-T5; ON: DE84001217
Country of Publication:
United States
Language:
English