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Analysis of sub-micron minral matter in coal via scanning transmission electron microscopy

Technical Report ·
OSTI ID:5320066
The fine-scale mineral matter in three US coals has been analyzed via scanning transmission electron microscopy (STEM). The samples observed were a North Dakota lignite, a Kentucky bituminous, and a Pennsylvania anthracite. Specific mineral types, differing among the three coals examined, appear to predominate at this fine size scale (particles less than or equal to 200nm in diameter). Fe-rich and Ba-rich minerals in the lignite, a Ti-rich mineral in the bituminous, and Ca-rich and Ti-rich minerals in the anthracite were the predominant species found. The inherent mineral content in the observed organic background also differs from coal to coal. The distributions of mineral species in the size range less than or equal to 200nm reported herein do not reflect the distributions in the larger size ranges obtained by more macroscopic techniques.
Research Organization:
Sandia National Labs., Livermore, CA (USA); Massachusetts Inst. of Tech., Cambridge (USA). Dept. of Materials Science and Engineering
DOE Contract Number:
AC04-76DP00789
OSTI ID:
5320066
Report Number(s):
SAND-82-8677; ON: DE82018614
Country of Publication:
United States
Language:
English

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