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Resistive and magnetic studies of Nd/sub 1/Ba/sub 2/Cu/sub 3/O/sub 7/. sqrt. /sub delta/ and Pr/sub 1/Ba/sub 2/Cu/sub 3/O/sub 7/. sqrt. /sub delta/

Journal Article · · Phys. Rev. B: Condens. Matter; (United States)

We report resistivity, structural, and magnetic susceptibility (chi/sup spin/(T)) measurements for the compounds Pr/sub 1/Ba/sub 2/Cu/sub 3/O/sub 7/..sqrt../sub delta/ and Nd/sub 1/Ba/sub 2/Cu/sub 3/O/sub 7/..sqrt../sub delta/. The Nd compound is superconducting with an onset transition temperature of 90 K, while the Pr compound is semiconducting above 4 K. The lattice parameters for these two materials have been determined using x-ray diffraction techniques, and both appear to be tetragonal, although the Nd/sub 1/Ba/sub 2/Cu/sub 3/O/sub 7/..sqrt../sub delta/ compound may exhibit some orthorhombic splitting. The high-temperature effective moments in the two systems are within a few percent of the free-ion moments. In each case the presence of significant curvature in the inverse susceptibility versus T behavior on the scale of 100 K suggests the presence of crystalline electric field splittings on the same energy scale. For the Pr compound this is further confirmed by a finite value for chi/sup spin/(0) and a residual large constant term at high temperatures. The possible origin of semiconducting behavior as compared with superconducting behavior in the Nd and other rare-earth compounds is discussed in terms of differences in charge-carrier density and possible role of valence fluctuations among Pr rare-earth ions

Research Organization:
Department of Physics, The Ohio State University, Columbus, Ohio 43210
OSTI ID:
5255443
Journal Information:
Phys. Rev. B: Condens. Matter; (United States), Journal Name: Phys. Rev. B: Condens. Matter; (United States) Vol. 37:13; ISSN PRBMD
Country of Publication:
United States
Language:
English

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