Alternate HNS I synthesis route via the intermediate dipicrylethane
A two step process for HNS synthesis consisting of the Shipp synthesis of dipicrylethane from TNT followed by the conversion of DPE to HNS by a Hungarian process was successfully demonstrated on a 50 g TNT scale. HNS yields of 60% and product purities of above 97% were obtained.
- Research Organization:
- Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (USA)
- DOE Contract Number:
- AC04-76DP00487
- OSTI ID:
- 5197226
- Report Number(s):
- MHSMP-78-56
- Country of Publication:
- United States
- Language:
- English
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Alternate HNS I synthesis route via the intermediate dipicrylethane
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