Synthesis of HNS I via the intermediate dipicrylethane: 5 kg scale
An alternate route for the synthesis of 2,2',4,4',6,6'-hexanitrostilbene has been successfully scaled to 5 kg quantities. The intermediate dipicrylethane was synthesized via the Shipp process and was subsequently oxidized into HNS through a Hungarian process.
- Research Organization:
- Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (USA)
- DOE Contract Number:
- AC04-76DP00487
- OSTI ID:
- 5197225
- Report Number(s):
- MHSMP-79-35
- Country of Publication:
- United States
- Language:
- English
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Alternate HNS I synthesis route via the intermediate dipicrylethane
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Related Subjects
45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
ALKANES
AROMATICS
CHEMICAL EXPLOSIVES
CHEMICAL REACTIONS
EXPLOSIVES
HYDROCARBONS
NITRO COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
RESEARCH PROGRAMS
STILBENE
SYNTHESIS
TNT
450100* -- Military Technology
Weaponry
& National Defense-- Chemical Explosions & Explosives
ALKANES
AROMATICS
CHEMICAL EXPLOSIVES
CHEMICAL REACTIONS
EXPLOSIVES
HYDROCARBONS
NITRO COMPOUNDS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
RESEARCH PROGRAMS
STILBENE
SYNTHESIS
TNT