Conversion of dimethyl ether--boron trifluoride complex to potassium fluoborate

Patent · Tue Jun 18 04:00:00 EDT 1957

OSTI ID:5093288

Eberle, A R

A method of preparing KBF/sub 4/ from the dimethyl ether complex of BF/sub 3/ is given. This may be accomplished by introducing the dimethyl ether complex of BF/sub 3/ into an aqueous solution of KF and alcohol, expelling the ether liberated from the complex by heating or stirring and recovering the KBF/sub 4/ so formed. The KBF/sub 4/ is then filtered from the alcohol-water solution, which may be recycled, to reduce the loss of KBF/sub 4/ which is not recovered by filtration.

• Assignee: Atomic Energy Commission
• Patent Number(s): US 2796323
• OSTI ID: 5093288
• Country of Publication: United States
• Language: English

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400201* -- Chemical & Physicochemical Properties
ALCOHOLS
ALKALI METAL COMPOUNDS
BORATES
BORIDES
BORON COMPLEXES
BORON COMPOUNDS
BORON FLUORIDES
CHEMICAL PREPARATION
COMPLEXES
ETHERS
FLUORIDES
FLUORINE COMPOUNDS
HALIDES
HALOGEN COMPOUNDS
HEATING
LOSSES
METHYL ETHER
ORGANIC COMPOUNDS
ORGANIC OXYGEN COMPOUNDS
POTASSIUM BORIDES
POTASSIUM COMPOUNDS
POTASSIUM FLUORIDES
PRECIPITATION
PREPARATION
RECOVERY
SEPARATION PROCESSES
SOLUTIONS
SYNTHESIS
WATER