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THE SODIUM HYDROXIDE-SODIUM HYDRIDE SYSTEM

Technical Report ·
DOI:https://doi.org/10.2172/4354764· OSTI ID:4354764

Portions of the NaOH-NaH phase diagram were studied by means of differential thermal analysis. Under certain conditions NaH will either react with NaOH according to the equation NaH + NaOH in equilibrium Na/sub 2/O + H/ sub 2/ or thermally dissociate according to the equation NaH in equilibrium Na + 1/2 H/sub 2/. Both of these reactions are suppressed by a high H/sub 2/ pressure; and NaH neither reacts nor dissociates to an extent sufficient to affect the results reported. This was evidenced by the fact that changing the H/ sub 2/ pressure above the system in the range indicated did not change, within the limit of error of the experiments ( approximately plus or minus 5 deg ), the temperature at which a phase change was started or completed. Therefore the concentrations of Na and Na/sub 2/O present in the samples must have been small in all cases. Under a high H/sub 2/ pressure, therefore, the system may be considered as essentiallybinary, consisting of NaOH and NaH. (auth)

Research Organization:
Metal Hydrides Inc. Metals Research Lab. , Beverly, Mass.
DOE Contract Number:
W-7405-ENG-26
NSA Number:
NSA-12-001209
OSTI ID:
4354764
Report Number(s):
CF-57-3-36
Country of Publication:
United States
Language:
English

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