Toward the development of high resolution synchrotron x-ray diffraction tomography of polycrystalline materials
- School of Materials Sci. & Eng., Georgia Institute of Technology, Atlanta, GA 30332-0245 (United States)
- SSRL, P.O. Box 4349, Bin 69, Stanford, CA 94309-0210 (United States)
In understanding the macroscopic response of polycrystalline structural materials to loading, it is frequently essential to know both the three-dimensional distribution of strain and of microtexture. The methods must be nondestructive, however, if the evolution of quantities, such as strain at a fatigue crack tip, are to be studied. This paper describes approaches for high resolution synchrotron x-ray diffraction tomography of polycrystalline materials. Preliminary experiments are reported on partially cracked compact tension samples of Al-Li 2090 and on model samples of randomly packed, millimeter-sized single crystals. Polychromatic beams collimated to diameters as small as 30 {mu}m have been used, and collecting the spatial distribution of diffracted intensity on image storage plates as a function of sample-to-detector separation allowed inference of the depth of the volume elements contributing to diffraction. The precision to which one can determine the depths of volume elements will be discussed as well approaches for three-dimensional, nondestructive strain mapping. {copyright} {ital 1996 American Institute of Physics.}
- OSTI ID:
- 434765
- Report Number(s):
- CONF-9510119--
- Journal Information:
- Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 9 Vol. 67; ISSN 0034-6748; ISSN RSINAK
- Country of Publication:
- United States
- Language:
- English
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