THE DETERMINATION OF FLUORIDE IN PLUTONIUM FLUORIDES
The Willard-Winter distillation was adapted to the determination of fluoride in plutonium fiuorides. Fluoride was distilled from samples in 12M sulfuric acid, and the distillate was then titrated to a visual end point with a standard solution of thorium nitrate. In the analysis of plutonium trifluoride the average recovery of fluoride was 98.6% of theoretical, and the standard deviation of the results was 1.3 relative%. (auth)
- Research Organization:
- Du Pont de Nemours (E.I.) & Co. Savannah River Lab., Augusta, Ga.
- NSA Number:
- NSA-12-005232
- OSTI ID:
- 4312760
- Report Number(s):
- DP-247
- Country of Publication:
- United States
- Language:
- English
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