Rapid solid-state synthesis of refractory nitrides
- Univ. of California, Los Angeles, CA (United States)
The authors describe a method for the rapid chemical preparation of refractory nitride compounds via solid state metathesis. Reaction of Li{sub 3}N and/or NaN{sub 3} and the corresponding metal halide is effective in producing TiN, ZrN, HfN, NbN, and TaN powders. X-ray diffraction, magnetic susceptibility, electron microscopy, thermal, and elemental analysis were all used in the characterization of these complexes. All the mononitrides crystallize in a cubic lattice.
- OSTI ID:
- 421010
- Journal Information:
- Inorganic Chemistry, Journal Name: Inorganic Chemistry Journal Issue: 25 Vol. 33; ISSN 0020-1669; ISSN INOCAJ
- Country of Publication:
- United States
- Language:
- English
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