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A PRECISE METHOD FOR DETERMINING VANADIUM IN ESSENTIALLY PURE VANADIUM METAL

Technical Report ·
OSTI ID:4190875

A method of analysis for vanadium in essentia1ly pure vanadium metal is presented. Precision resulting in a limit of error (0.95) for a single determination of plus or minus O.O79% is achieved by oxidizing the weighed and dissolved sample to vanadium(V) and reacting this solution with a weighed slight excess of ferrous ammonium sulfate hexahydrate. The excess reagent is then back- titrated with standard potassium dichromate solution, the titration representing less than 1% of the amount of vanadium present. (auth)

Research Organization:
Union Carbide Nuclear Co. Y-12 Plant, Oak Ridge, Tenn.
DOE Contract Number:
W-7405-ENG-26
NSA Number:
NSA-14-013688
OSTI ID:
4190875
Report Number(s):
Y-1294
Country of Publication:
United States
Language:
English

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