THE ANALYSIS OF SOME VOLATILE PHOSPHORUS COMPOUNDS BY GAS-LIQUID CHROMATOGRAPHY. Includes Papers: GAS CHROMATOGRAPHIC ANALYSIS OF SOME VOLATILE PHOSPHORUS COMPOUNDS. REACTIONS OF TRITIUM ATOMS WITH FROZEN HYDROCARBONS
Technical Report
·
OSTI ID:4161556
In the first paper, a gas chromatographic method for the analysis of mixtures of (CH/sub 3/O)/sub 2/POH - (C/sub 2/H/sub 5/O)/sub 2/POH, PC1/sub 3/ PSC1/sub 3, and PC13/ - POC1/sub 3/ was developed. Pyrex glass was used as the column and body of the thermal conductivity cell, and tantalum wire was employed for the sensing elements. In the second paper, tritium atoms generated from molecular hydrogen at a tungsten filament at 1750 deg C were reacted with the following frozen compounds: benzene, cyclohexane, cyclohexene, 1 -hexene, and n- hexane, Both addition and substitution were observed with unsaturated compounds. With saturated compounds, substitution was the principle reaction that occurred. (C.J.G.)
- Research Organization:
- Kansas State Univ., Manhattan
- NSA Number:
- NSA-15-001320
- OSTI ID:
- 4161556
- Report Number(s):
- TID-6437
- Country of Publication:
- United States
- Language:
- English
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