GAS CHROMATOGRAPHIC ANALYSIS OF SOME VOLATILE PHOSPHORUS COMPOUNDS
Journal Article
·
· Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed.
A rapid gas chromatographic method of analysis for mixtures of phosphorus trichloride-thiophosphoryl chloride, phosphorus trichloride - phosphoryl chloride, and dionethyl phosphite -diethyl phosphite was developed. The area per cent of each peak of the chromatogram closely agreed with the weight per cent of the corresponding component of the mixture. The column and detector used with the reactive inorganic compounds were constructed from inert materials. Described is a simple, yet dependable, thermal conductivity cell made from borosilicate glass with tantalum filaments. (auth)
- Research Organization:
- Kansas State Univ., Manhattan
- Sponsoring Organization:
- USDOE
- NSA Number:
- NSA-15-014213
- OSTI ID:
- 4053514
- Journal Information:
- Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed., Journal Name: Analytical Chemistry (U.S.) Formerly Ind. Eng. Chem., Anal. Ed. Vol. Vol: 33; ISSN ANCHA
- Country of Publication:
- Country unknown/Code not available
- Language:
- English
Similar Records
THE ANALYSIS OF SOME VOLATILE PHOSPHORUS COMPOUNDS BY GAS-LIQUID CHROMATOGRAPHY. Includes Papers: GAS CHROMATOGRAPHIC ANALYSIS OF SOME VOLATILE PHOSPHORUS COMPOUNDS. REACTIONS OF TRITIUM ATOMS WITH FROZEN HYDROCARBONS
Electrochemical cell utilizing a mixture of phosphorus oxychloride and a low freezing solvent as the electrolyte
Phosphorylation of halogen-substituted. beta. -dicarbonyl compounds with phosphorus chloride in presence of triethylamine
Technical Report
·
Thu Dec 31 23:00:00 EST 1959
·
OSTI ID:4161556
Electrochemical cell utilizing a mixture of phosphorus oxychloride and a low freezing solvent as the electrolyte
Patent
·
Tue Oct 09 00:00:00 EDT 1984
·
OSTI ID:6018908
Phosphorylation of halogen-substituted. beta. -dicarbonyl compounds with phosphorus chloride in presence of triethylamine
Journal Article
·
Sun Sep 20 00:00:00 EDT 1987
· J. Gen. Chem. USSR (Engl. Transl.); (United States)
·
OSTI ID:5129273