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Results of the first provisional technical secretariat interlaboratory comparison test

Conference ·
OSTI ID:416152
;  [1]
  1. Army Edgewood Research, Army Material Command Treaty Lab., Aberdeen Proving Ground, MD (United States)

The principal task of this laboratory in the first Provisional Technical Secretariat (PTS) Interlaboratory Comparison Test was to verify and test the extraction and preparation procedures outlined in the Recommended Operating Procedures for Sampling and Analysis in the Verification of Chemical Disarmament in addition to our laboratory extraction methods and our laboratory analysis methods. Sample preparation began on 16 May 1994 and analysis was completed on 12 June 1994. The analytical methods used included NMR ({sup 1}H and {sup 31}P) GC/AED, GC/MS (EI and methane CI), GC/IRD, HPLC/IC, HPLC/TSP/MS, MS/MS(Electrospray), and CZE.

Research Organization:
Oak Ridge National Lab., TN (United States)
OSTI ID:
416152
Report Number(s):
ORNL/M--4315; CONF-9409370--; ON: DE95016127
Country of Publication:
United States
Language:
English

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