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U.S. Department of Energy
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AN AQUA REGIA FLOWSHEET FOR URANIUM DISSOLUTION

Technical Report ·
OSTI ID:4160825
A dilute aqua regia flowsheet for the complete dissolution of solid uranium slugs in 7.5 hours is shown. Before the dissolver product solution can be further prooessed in stainiess steel equipment, the chloride must be removed. Two flowsheets for chloride removal are presented. In the first flowsheet, the chloride is removed by volatilization and in the second, by oxidation. The chloride removal need not be carried out in the dissolver vessel. The larger safe batch sizes of a homogeneous system may permit combining several batches from the heterogeneous dissolver system before chloride removal. Titanium, Haynes 25, and Hastelloy F are possible materials of construction for the process equipment that is to contain both nitric and hydrochloric acids. (auth)
Research Organization:
General Electric Co. Hanford Atomic Products Operation, Richland, Wash.
DOE Contract Number:
AT(45-1)-1350
NSA Number:
NSA-14-017840
OSTI ID:
4160825
Report Number(s):
HW-61048
Country of Publication:
United States
Language:
English

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