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Title: Manifestations of dynamic strain aging in soft-oriented NiAl single crystals

Journal Article · · Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science
DOI:https://doi.org/10.1007/BF02595446· OSTI ID:413286
;  [1];  [2]
  1. Univ. of Florida, Gainesville, FL (United States). Dept. of Materials Science and Engineering
  2. NASA-Lewis Research Center, Cleveland, OH (United States). Materials Div.

The tensile and compressive properties of six NiAl-base single-crystal alloys have been investigated at temperatures between 77 and 1,200 K. The normalized critical resolved shear stresses (CRSS/E) and work-hardening rates ({theta}/E) for these alloys generally decreased with increasing temperature. However, anomalous peaks or plateaus for these properties were observed in conventional purity (CPNiAl), Si-doped (NiAl-Si), C-doped low Si (UF-NiAl1), and Mo-doped (NiAl-Mo) alloys at intermediate temperatures (600 to 1,000 K). This anomalous behavior was not observed in high-purity, low interstitial material (HP-NiAl). Low or negative strain-rate sensitivities (SRS) also were observed in all six alloys in this intermediate temperature range. Coincident with the occurrence of negative strain-rate sensitivities was the observation of serrated stress-strain curves in the CPNiAl and NiAl-Si alloys. These phenomena have been attributed to dynamic strain aging (DSA). The corresponding dislocation microstructures at low temperatures (300 to 600 K) were composed of well-defined cells. At intermediate temperatures (600 to 900 K), either poorly defined cells or coarse bands of localized slip, reminiscent of the vein structures observed in low-cycle fatigue specimens deformed in the DSA regime, were observed in conventional purity, Si-doped, and in Mo-doped alloys. In contrast, a well-defined cell structure persisted in the low interstitial, high-purity alloy. At elevated temperatures ({ge}1,000 K), more uniformly distributed dislocations and sub-boundaries were observed in all alloys. These observations are consistent with the occurrence of DSA in NiAl single-crystal alloys at intermediate temperatures.

Sponsoring Organization:
National Aeronautics and Space Administration, Washington, DC (United States)
OSTI ID:
413286
Journal Information:
Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science, Vol. 27, Issue 11; Other Information: PBD: Nov 1996
Country of Publication:
United States
Language:
English