ANALYTICAL METHOD FOR THE DETERMINATION OF ZIRCONIUM METAL IN IGNITED URANIUM/ZIRCONIUM RESIDUES
Technical Report
·
OSTI ID:4086414
The sample is treated with a solution of bromine in ethyl acetate in which zirconium metal is soluble. After filtration the filtrate is evaporated to dryness and the residue redissolved in acid. Zirconium in separated from uranium by precipitation with mandelic acid, and determined volumetrically in a sulphuric acid solution using standard E.D.T.A. and bismuth solutions. The method is applicable to samples containing 0.1 to 20% w/w zirconium metal in combination with uranlum metal or oxides. The determination of zirconium has shown a coefficient of variation of plus or minus 0.6% at the 40 mg Zr level. (auth)
- Research Organization:
- United Kingdom Atomic Energy Authority. Production Group, Springfields, Lancs, England
- NSA Number:
- NSA-18-013640
- OSTI ID:
- 4086414
- Report Number(s):
- PG-Report-515
- Country of Publication:
- Country unknown/Code not available
- Language:
- English
Similar Records
ANALYTICAL METHOD FOR THE VOLUMETRIC DETERMINATION OF ZIRCONIUM IN URANIUM/ ZIRCONIUM MASTER ALLOY
TENTATIVE METHOD FOR THE DETERMINATION OF COBALT AS AN IMPURITY IN ZIRCONIUM AND ZIRCALOY
THE VOLUMETRIC DETERMINATION OF ZIRCONIUM IN URANIUM-ZIRCONIUM MASTER ALLOY
Technical Report
·
Sun Dec 31 23:00:00 EST 1961
·
OSTI ID:4798384
TENTATIVE METHOD FOR THE DETERMINATION OF COBALT AS AN IMPURITY IN ZIRCONIUM AND ZIRCALOY
Technical Report
·
Sun Jan 27 23:00:00 EST 1957
·
OSTI ID:4328809
THE VOLUMETRIC DETERMINATION OF ZIRCONIUM IN URANIUM-ZIRCONIUM MASTER ALLOY
Technical Report
·
Sat Feb 28 23:00:00 EST 1959
·
OSTI ID:4211830