CHEMICAL SYNTHESIS OF TRITIUM-LABELED LINOLEIC ACID
Tritium-labeled linoleic acid with a specific activity of 357 mC/mmole was obtained in 70% yield from totally synthesized octadeca-9,12-diynoic acid. A source of 1 curie of tritium gas was used to semihydrogenate the diacetylenic acid in the presence of Lindlar's catalyst. Chemical and radiochemical purity of the final product were assessed by chromatographic methods. Evidence from mild oxidation indicated that the tritium-labeled linoleic acid was prepared with a specificity of greater than 95% of the activity at the
- Research Organization:
- Univ. of Illinois, Urbana
- Sponsoring Organization:
- USDOE
- NSA Number:
- NSA-18-016070
- OSTI ID:
- 4067997
- Journal Information:
- Biochemistry (U.S.), Journal Name: Biochemistry (U.S.) Vol. Vol: 3; ISSN BICHA
- Country of Publication:
- Country unknown/Code not available
- Language:
- English
Similar Records
EXPERIMENTS ON TRITIUM-LABELED INSULIN
Analysis and chromatographic purification of eicosanoids multiply labeled by tritium
A METHOD OF TRITIUM LABELING
Technical Report
·
Fri Oct 30 23:00:00 EST 1959
·
OSTI ID:4293356
Analysis and chromatographic purification of eicosanoids multiply labeled by tritium
Journal Article
·
Sat Dec 31 23:00:00 EST 1988
· Sov. Radiochem. (Engl. Transl.); (United States)
·
OSTI ID:5912753
A METHOD OF TRITIUM LABELING
Journal Article
·
Fri Jun 01 00:00:00 EDT 1962
· Journal of Organic Chemistry (U.S.)
·
OSTI ID:4713760