A NEW COMPLEX COMPOUND OF RHENIUM
Journal Article
·
· J. Ind. Chem. Soc.
OSTI ID:4062994
A method is outlined for the preparation of a new complex compound of rhenium, STARe(OH)/sub 2/Cl/sub 2/DPO!/sub x/, where DPO is a molecule of diphenylcarbazone less one H atom. In this method, an acetone solution of diphenylcarbazide is added slowly to an ice solution of potassium perrhenate solution in 8 N HCl to precipitate deep violet solids, which are separated, redissolved, re-precipitated, and dried in vacuum. The value of x was determined from freezing point depressions to be 0.88, which suggests the formula Re(OH)/sub 2/Cl/sub 2/DPO for the complex. The absorption spectrum of the complex is reported. (D.L.C.)
- Research Organization:
- Gujarat Coll., Ahmedabad, India; and Inst. of Science, Bombay
- NSA Number:
- NSA-15-014203
- OSTI ID:
- 4062994
- Journal Information:
- J. Ind. Chem. Soc., Journal Name: J. Ind. Chem. Soc. Vol. Vol: 37
- Country of Publication:
- Country unknown/Code not available
- Language:
- English
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