THE DETERMINATION OF TRACES OF OSMIUM AND IRIDIUM IN SAMPLES OF PALLADIUM AND PLATINUM BY NEUTRON-ACTIVATION ANALYSIS

Journal Article · Wed Feb 01 04:00:00 EST 1961 · Talanta (England)

DOI:https://doi.org/10.1016/0039-9140(61)80047-7· OSTI ID:4039877

Morris, D F.C.; Killick, R A

A method is described for the determination of ultramicro quantities o-f osmium and iridium in samples of palladium and platinum. In order to avoid self- shielding differences between samples and standards during neutron irradiation, standards are prepared by the addition of very small kown amounts of osmium and iridium to analytical samples. In the analysis of palladium samples the Harwell Pile BEPO is used as the neutron source. To avoid spurious results due (n,p) and (n, alpha ) reactions, the Pile DIDO has had to be used for neutron-activation of samples of platinum. Each determination requires 0.1 g of sample, and radiochemical separations using carriers are used to isolate the induced osmium and iridium activities. Results are quoted for the osmium and iridium contents of some pure palladium and platinum samples. (auth)

• Research Organization: Brunel Coll. of Tech., London
• NSA Number: NSA-15-015579
• OSTI ID: 4039877
• Journal Information: Talanta (England), Journal Name: Talanta (England) Vol. Vol: 8; ISSN TLNTA
• Country of Publication: Country unknown/Code not available
• Language: English

Related Subjects

ACTIVATION ANALYSIS
BEPO
CHEMISTRY
COUPLING
DECAY
ELECTRODYNAMICS
FIELD THEORY
INTERACTIONS
IRIDIUM
KAONS
MUONS
NEUTRON SOURCES
NEUTRONS
OSMIUM
PALLADIUM
PHOTONS
PLATINUM
PREPARATION
QUANTITATIVE ANALYSIS
QUANTUM ELECTRODYNAMICS
QUANTUM MECHANICS
RESEARCH REACTORS
SAMPLING
STANDARDS
TENSORS
TRITIUM
VECTORS