Cleaning and outgassing studies of machinable tungsten for beamline safety shutters
- Experimental Facilities Division, Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439 (United States)
Machinable tungsten blocks are used as safety shutters in the front ends and the beamlines at the Advanced Photon Source (APS). The machinable tungsten used is characterized as a UHV-compatible metal by the vendor and was developed through a joint research effort with the APS. However, because of the inherent porosity in the sintered tungsten metal, it may present a vacuum problem and has to be subjected to strict vacuum testing before it is put on the beamlines. We have chosen specially heat-treated machinable tungsten with a density of 18 g/cm{sup 3} for safety shutters. In-house-developed, environmentally friendly vacuum cleaning procedures were used. In this paper, we present results of thermal outgassing tests for machinable tungsten safety shutter sets. Each set consists of five blocks and has a total area of 4500 cm{sup 2}. A cleaning procedure using alkaline detergent ultrasonic washes, deionized water rinses, and a 500{degree}C vacuum furnace baking was used before outgassing measurements. Outgassing rates 10 hours after initial pump down at room temperature reached {approximately}1.60{times}10{sup {minus}10} Torr{center_dot}l{center_dot}s{sup {minus}1}{center_dot}cm{sup {minus}2} for machinable tungsten and {approximately}1.56{times}10{sup {minus}10} Torr{center_dot}l{center_dot}s{sup {minus}1}{center_dot}cm{sup {minus}2} for the stainless steel vacuum chamber. The outgassing rate of machinable tungsten 24 hours after an {ital in} {ital situ} 48 h bake at 160{degree}C is also comparable to that of the stainless steel vacuum chamber. The importance of a 500{degree}C vacuum furnace baking has been confirmed by outgassing studies for machinable tungsten sets that were not subject to vacuum furnace baking. {copyright} {ital 1996 American Institute of Physics.}
- Research Organization:
- Argonne National Laboratory (ANL), Argonne, IL
- DOE Contract Number:
- W-31109-ENG-38
- OSTI ID:
- 389646
- Report Number(s):
- CONF-9510119--
- Journal Information:
- Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 9 Vol. 67; ISSN 0034-6748; ISSN RSINAK
- Country of Publication:
- United States
- Language:
- English
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