Specimen preparation for x-ray fluorescence analysis of solutions

Journal Article · Sun Dec 31 00:00:00 EST 1995 · Advances in X-Ray Analysis

DOI:https://doi.org/10.1007/978-1-4615-1797-9_89· OSTI ID:369877

Eksperiandova, L P; Spolnik, Z M; Blank, A B; Aliseychik, B B ^[1]

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1. Inst. for Single Crystals, Kharkov (Ukraine)

Specimens for x-ray fluorescence analysis (XRFA) were prepared by adding dry gelatine (10%) to the analysis solution, homogenizing the mixture and cooling for 20 minutes. Thus, a compact resilient mass could be formed with the required shape and size; the roughness of the surface was determined by the roughness of the surface on which the specimen was formed, much the same as highly polished. Various calibration methods can be applied in the XRFA of a variety of materials if such specimens are used. 12 refs., 1 fig., 2 tabs.

• Sponsoring Organization: USDOE
• OSTI ID: 369877
• Report Number(s): CONF-9408178-; ISSN 0376-0308; TRN: 96:004756-0081
• Journal Information: Advances in X-Ray Analysis, Vol. 38; Conference: 43. annual Denver x-ray conference on applications of x-ray analysis, Steamboat Spring, CO (United States), 1-5 Aug 1994; Other Information: PBD: 1995
• Country of Publication: United States
• Language: English

Related Subjects

66 PHYSICS
40 CHEMISTRY
X-RAY FLUORESCENCE ANALYSIS
SAMPLE PREPARATION
SOLUTIONS
CALIBRATION