Specimen preparation for x-ray fluorescence analysis of solutions

Journal Article · Sat Dec 30 23:00:00 EST 1995 · Advances in X-Ray Analysis

DOI:https://doi.org/10.1007/978-1-4615-1797-9_89· OSTI ID:369877

Eksperiandova, L P; Spolnik, Z M; Blank, A B; Aliseychik, B B ^[1]

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1. Inst. for Single Crystals, Kharkov (Ukraine)

Specimens for x-ray fluorescence analysis (XRFA) were prepared by adding dry gelatine (10%) to the analysis solution, homogenizing the mixture and cooling for 20 minutes. Thus, a compact resilient mass could be formed with the required shape and size; the roughness of the surface was determined by the roughness of the surface on which the specimen was formed, much the same as highly polished. Various calibration methods can be applied in the XRFA of a variety of materials if such specimens are used. 12 refs., 1 fig., 2 tabs.

• Sponsoring Organization: USDOE
• OSTI ID: 369877
• Report Number(s): CONF-9408178--
• Journal Information: Advances in X-Ray Analysis, Journal Name: Advances in X-Ray Analysis Vol. 38; ISSN 0376-0308; ISSN AXRAAA
• Country of Publication: United States
• Language: English

Related Subjects

40 CHEMISTRY
66 PHYSICS
CALIBRATION
SAMPLE PREPARATION
SOLUTIONS
X-RAY FLUORESCENCE ANALYSIS