Externally Heated Diamond ANvil Cell Experimentation (EH-DANCE) for studying materials and processes under extreme conditions

Wang, Siheng; Berrada, Meryem; Chao, Keng-Hsien; Lai, Xiaojing; Zhu, Feng; Zhang, Dongzhou; Chariton, Stella; Prakapenka, Vitali B.; Sinogeikin, Stanislav; Chen, Bin

doi:10.1063/5.0180103

Externally Heated Diamond ANvil Cell Experimentation (EH-DANCE) for studying materials and processes under extreme conditions (in EN)

Journal Article · Tue Dec 05 23:00:00 EST 2023 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/5.0180103· OSTI ID:2578446

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University of Hawaii at Manoa, Honolulu, HI (United States)
University of Hawaii at Manoa, Honolulu, HI (United States); China University of Geosciences (Wuhan) (CUG), (China)
University of Hawaii at Manoa, Honolulu, HI (United States); University of Chicago, IL (United States). Center for Advanced Radiation Sources (CARS)
University of Chicago, IL (United States). Center for Advanced Radiation Sources (CARS)
DAC Tools, LLC, Naperville, IL (United States)

Externally heated diamond anvil cells provide a stable and uniform thermal environment, making them a versatile device to simultaneously generate high-pressure and high-temperature conditions in various fields of research, such as condensed matter physics, materials science, chemistry, and geosciences. The present study features the Externally Heated Diamond ANvil Cell Experimentation (EH-DANCE) system, a versatile configuration consisting of a diamond anvil cell with a customized microheater for stable resistive heating, bidirectional pressure control facilitated by compression and decompression membranes, and a water-cooled enclosure suitable for vacuum and controlled atmospheres. This integrated system excels with its precise control of both pressure and temperature for mineral and materials science research under extreme conditions. Here, we showcase the capabilities of the system through its successful application in the investigation of the melting temperature and thermal equation of state of high-pressure ice-VII at temperatures up to 1400 K. The system was also used to measure the elastic properties of solid ice-VII and liquid H₂O using Brillouin scattering and Raman spectra of carbonates using Raman spectroscopy, highlighting the potential of the EH-DANCE system in high-pressure research.

View Accepted Manuscript (DOE)

Research Organization:: University of Chicago, IL (United States); Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities (SUF); USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division (CSGB); National Science Foundation (NSF); National Natural Science Foundation of China (NSFC)

Grant/Contract Number:: AC02-06CH11357; FG02-94ER14466

OSTI ID:: 2578446

Journal Information:: Review of Scientific Instruments, Journal Name: Review of Scientific Instruments Journal Issue: 12 Vol. 94; ISSN 1089-7623; ISSN 0034-6748

Publisher:: AIP PublishingCopyright Statement

Country of Publication:: United States

Language:: EN

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