The ability to remotely control pressure in diamond anvil cells (DACs) in accurate and consistent manner at room temperature, as well as at cryogenic and elevated temperatures, is crucial for effective and reliable operation of a high-pressure synchrotron facility such as High Pressure Collaborative Access Team (HPCAT). Over the last several years, a considerable effort has been made to develop instrumentation for remote and automated pressure control in DACs during synchrotron experiments. We have designed and implemented an array of modular pneumatic (double-diaphragm), mechanical (gearboxes), and piezoelectric devices and their combinations for controlling pressure and compression/decompression rate at various temperature conditions from 4 K in cryostats to several thousand Kelvin in laser-heated DACs. Because HPCAT is a user facility and diamond cells for user experiments are typically provided by users, our development effort has been focused on creating different loading mechanisms and frames for a variety of existing and commonly used diamond cells rather than designing specialized or dedicated diamond cells with various drives. In this paper, we review the available instrumentation for remote static and dynamic pressure control in DACs and show some examples of their applications to high pressure research.
Smith, Jesse S., et al. "Online remote control systems for static and dynamic compression and decompression using diamond anvil cells." Review of Scientific Instruments, vol. 86, no. 7, Jul. 2015. https://doi.org/10.1063/1.4926892
Smith, Jesse S., Rod, Eric, Lin, Chuanlong, Kenney-Benson, Curtis, & Shen, Guoyin (2015). Online remote control systems for static and dynamic compression and decompression using diamond anvil cells. Review of Scientific Instruments, 86(7). https://doi.org/10.1063/1.4926892
Smith, Jesse S., Rod, Eric, Lin, Chuanlong, et al., "Online remote control systems for static and dynamic compression and decompression using diamond anvil cells," Review of Scientific Instruments 86, no. 7 (2015), https://doi.org/10.1063/1.4926892
@article{osti_22482697,
author = {Smith, Jesse S. and Rod, Eric and Lin, Chuanlong and Kenney-Benson, Curtis and Shen, Guoyin},
title = {Online remote control systems for static and dynamic compression and decompression using diamond anvil cells},
annote = {The ability to remotely control pressure in diamond anvil cells (DACs) in accurate and consistent manner at room temperature, as well as at cryogenic and elevated temperatures, is crucial for effective and reliable operation of a high-pressure synchrotron facility such as High Pressure Collaborative Access Team (HPCAT). Over the last several years, a considerable effort has been made to develop instrumentation for remote and automated pressure control in DACs during synchrotron experiments. We have designed and implemented an array of modular pneumatic (double-diaphragm), mechanical (gearboxes), and piezoelectric devices and their combinations for controlling pressure and compression/decompression rate at various temperature conditions from 4 K in cryostats to several thousand Kelvin in laser-heated DACs. Because HPCAT is a user facility and diamond cells for user experiments are typically provided by users, our development effort has been focused on creating different loading mechanisms and frames for a variety of existing and commonly used diamond cells rather than designing specialized or dedicated diamond cells with various drives. In this paper, we review the available instrumentation for remote static and dynamic pressure control in DACs and show some examples of their applications to high pressure research.},
doi = {10.1063/1.4926892},
url = {https://www.osti.gov/biblio/22482697},
journal = {Review of Scientific Instruments},
issn = {ISSN RSINAK},
number = {7},
volume = {86},
place = {United States},
year = {2015},
month = {07}}