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A comparison study on the densification behavior and mechanical properties of gelcast vs conventionally formed B{sub 4}C sintered conventionally and by microwaves

Technical Report ·
DOI:https://doi.org/10.2172/244628· OSTI ID:244628
;  [1]; ;  [2]
  1. Oak Ridge National Lab., TN (United States)
  2. Y-12 Development Div., Oak Ridge, TN (United States)

The utilization of microwave energy for reaching high temperatures necessary to densify B{sub 4}C powder is compared with conventional means of sintering by evaluating the mechanical properties after densification. Microwave energy has been shown to be an effective means for achieving high sintered densities, even though temperatures of {approximately} 2,250 C are required. In this study, green preforms of B{sub 4}C specimens were sintered by both conventional and microwave heating. This study also utilized an advanced forming method called ``Gelcasting`` developed at ORNL. Gelcasting is a fluid forming process whereby high solids suspensions of powders containing dissolved monomers are cast into a mold, then polymerized or ``gelled`` in situ. This investigation compares microstructures and mechanical properties of both Gelcast B{sub 4}C and ``conventionally`` die-pressed B{sub 4}C. The microstructures and final mechanical properties of B{sub 4}C specimens are discussed.

Research Organization:
Oak Ridge National Lab., TN (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC05-96OR22464
OSTI ID:
244628
Report Number(s):
CONF-960401--35; ON: DE96010670
Country of Publication:
United States
Language:
English

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