X-ray spectrometer and methods for use

Seidler, Gerald Todd; Hoidn, Oliver; Holden, William

X-ray spectrometer and methods for use

Patent · Tue Oct 24 00:00:00 EDT 2023

OSTI ID:2293758

Seidler, Gerald Todd; Hoidn, Oliver; Holden, William

A spectrometer includes a crystal analyzer having a radius of curvature that defines a Rowland circle, a sample stage configured to support a sample such that the sample is offset from the Rowland circle, x-ray source configured to emit unfocused x-rays toward the sample stage, and a position-sensitive detector that is tangent to the Rowland circle. A method performed via a spectrometer includes emitting, via an x-ray source, unfocused x-rays toward a sample that is mounted on a sample stage such that the sample is offset from the Rowland Circle, thereby causing the sample to emit x-rays that impinge on the crystal analyzer or transmit a portion of the unfocused x-rays to impinge on the crystal analyzer; scattering, via the crystal analyzer, the x-rays that impinge on the crystal analyzer; and detecting the scattered x-rays via a position-sensitive detector that is tangent to the Rowland circle.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States); Univ. of Washington, Seattle, WA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC52-06NA25396; SC0002194; SC0008580

Assignee:: University of Washington (Seattle, WA)

Patent Number(s):: 11,796,490

Application Number:: 17/366,759

OSTI ID:: 2293758

Country of Publication:: United States

Language:: English

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A novel von Hamos spectrometer for efficient X-ray emission spectroscopy in the laboratory Anklamm, Lars; Schlesiger, Christopher; Malzer, Wolfgang Review of Scientific Instruments, Vol. 85, Issue 5 https://doi.org/10.1063/1.4875986	journal	May 2014
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Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J. Structural Dynamics, Vol. 2, Issue 2 https://doi.org/10.1063/1.4913585	journal	March 2015
Note: A disposable x-ray camera based on mass produced complementary metal-oxide-semiconductor sensors and single-board computers Hoidn, Oliver R.; Seidler, Gerald T. Review of Scientific Instruments, Vol. 86, Issue 8 https://doi.org/10.1063/1.4929713	journal	August 2015
Energy-dispersive X-ray emission spectroscopy using an X-ray free-electron laser in a shot-by-shot mode Alonso-Mori, R.; Kern, J.; Gildea, R. J. Proceedings of the National Academy of Sciences, Vol. 109, Issue 47, p. 19103-19107 https://doi.org/10.1073/pnas.1211384109	journal	November 2012
Variation of Ti Valence with Lithium Content in Lithiated/Delithiated Li ₄ Ti ₅ O ₁₂ Studied by X-Ray Absorption near the Edge Structure Yu, Peng-Fei; Cui, Zhong-Hui; Meng, Jian-Wei Chinese Physics Letters, Vol. 30, Issue 3 https://doi.org/10.1088/0256-307X/30/3/036102	journal	March 2013
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A Modern Laboratory XAFS Cookbook Seidler, Gt; Mortensen, Dr; Ditter, As Journal of Physics: Conference Series, Vol. 712 https://doi.org/10.1088/1742-6596/712/1/012015	journal	May 2016
Benchtop Nonresonant X-ray Emission Spectroscopy: Coming Soon to Laboratories and XAS Beamlines Near You? Mortensen, Devon R.; Seidler, Gerald T.; Ditter, Alexander S. Journal of Physics: Conference Series, Vol. 712 https://doi.org/10.1088/1742-6596/712/1/012036	journal	May 2016
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X-ray absorption spectroscopy study of the Li _x FePO ₄ cathode during cycling using a novel electrochemical in situ reaction cell Deb, Aniruddha; Bergmann, Uwe; Cairns, Elton J. Journal of Synchrotron Radiation, Vol. 11, Issue 6 https://doi.org/10.1107/S0909049504024641	journal	October 2004
A new X-ray spectrometer with large focusing crystal analyzer Welter, Edmund; Machek, Pavel; Dräger, Günter Journal of Synchrotron Radiation, Vol. 12, Issue 4 https://doi.org/10.1107/S0909049505007843	journal	June 2005
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A 2 m inelastic X-ray scattering spectrometer at CMC-XOR, Advanced Photon Source Hill, J. P.; Coburn, D. S.; Kim, Y. -J. Journal of Synchrotron Radiation, Vol. 14, Issue 4 https://doi.org/10.1107/S0909049507018006	journal	June 2007
A versatile in situ spectroscopic cell for fluorescence/transmission EXAFS and X-ray diffraction of heterogeneous catalysts in gas and liquid phase Hannemann, Stefan; Casapu, Maria; Grunwaldt, Jan-Dierk Journal of Synchrotron Radiation, Vol. 14, Issue 4 https://doi.org/10.1107/S0909049507024466	journal	June 2007
High-resolution spectroscopy on an X-ray absorption beamline Hazemann, Jean-Louis; Proux, Olivier; Nassif, Vivian Journal of Synchrotron Radiation, Vol. 16, Issue 2 https://doi.org/10.1107/S0909049508043768	journal	January 2009
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New developments in fabrication of high-energy-resolution analyzers for inelastic X-ray spectroscopy Said, Ayman H.; Sinn, Harald; Divan, Ralu Journal of Synchrotron Radiation, Vol. 18, Issue 3 https://doi.org/10.1107/S0909049511001828	journal	March 2011
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Improving the energy resolution of bent crystal X-ray spectrometers with position-sensitive detectors Honkanen, Ari-Pekka; Verbeni, Roberto; Simonelli, Laura Journal of Synchrotron Radiation, Vol. 21, Issue 4 https://doi.org/10.1107/S1600577514011163	journal	June 2014
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Simple solutions for spectroscopic, photon counting X-ray imaging detectors Nachtra, F.; Hofmann, T.; Firsching, M. 2009 IEEE Nuclear Science Symposium and Medical Imaging Conference (NSS/MIC 2009), 2009 IEEE Nuclear Science Symposium Conference Record (NSS/MIC) https://doi.org/10.1109/NSSMIC.2009.5402242	conference	October 2009
Experimental and Theoretical Evaluation of a High Resolution CMOS Based Detector Under X-Ray Imaging Conditions Michail, Christos M.; Spyropoulou, Vasiliki A.; Fountos, George P. IEEE Transactions on Nuclear Science, Vol. 58, Issue 1 https://doi.org/10.1109/TNS.2010.2094206	journal	February 2011
Critical review: Effects of complex interactions on structure and dynamics of supported metal catalysts Frenkel, Anatoly I.; Cason, Michael W.; Elsen, Annika Journal of Vacuum Science & Technology A: Vacuum, Surfaces, and Films, Vol. 32, Issue 2 https://doi.org/10.1116/1.4820493	journal	March 2014
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Structure and Electrochemical Properties of LiFe[sub x]Mn[sub 2−x]O[sub 4] (0≤x≤0.5) Spinel as 5 V Electrode Material for Lithium Batteries Shigemura, H.; Sakaebe, H.; Kageyama, H. Journal of The Electrochemical Society, Vol. 148, Issue 7 https://doi.org/10.1149/1.1377593	journal	January 2001
Synthesis, Cation Distribution, and Electrochemical Properties of Fe-Substituted Li[sub 2]MnO[sub 3] as a Novel 4 V Positive Electrode Material Tabuchi, Mitsuharu; Nakashima, Akiko; Shigemura, Hikari Journal of The Electrochemical Society, Vol. 149, Issue 5 https://doi.org/10.1149/1.1462791	journal	January 2002
Investigation of the Local Structure of the LiNi[sub 0.5]Mn[sub 0.5]O[sub 2] Cathode Material during Electrochemical Cycling by X-Ray Absorption and NMR Spectroscopy Yoon, Won-Sub; Paik, Younkee; Yang, Xiao-Qing Electrochemical and Solid-State Letters, Vol. 5, Issue 11 https://doi.org/10.1149/1.1513001	journal	January 2002
Study of the Capacity Fading Mechanism for Fe-Substituted LiCoO[sub 2] Positive Electrode McLaren, Victoria L.; West, Anthony R.; Tabuchi, Mitsuharu Journal of The Electrochemical Society, Vol. 151, Issue 5 https://doi.org/10.1149/1.1688796	journal	January 2004
In Situ X-Ray Absorption Spectroscopic Study of Li[sub 1.05]Ni[sub 0.35]Co[sub 0.25]Mn[sub 0.4]O[sub 2] Cathode Material Coated with LiCoO[sub 2] Deb, Aniruddha; Bergmann, Uwe; Cramer, Stephen P. Journal of The Electrochemical Society, Vol. 154, Issue 6 https://doi.org/10.1149/1.2720762	journal	January 2007
An Electrochemical Cell for Operando Study of Lithium Batteries Using Synchrotron Radiation Leriche, J. B.; Hamelet, S.; Shu, J. Journal of The Electrochemical Society, Vol. 157, Issue 5 https://doi.org/10.1149/1.3355977	journal	January 2010
Review of LiFePO ₄ Phase Transition Mechanisms and New Observations from X-ray Absorption Spectroscopy Love, Corey T.; Korovina, Anna; Patridge, Christopher J. Journal of The Electrochemical Society, Vol. 160, Issue 5 https://doi.org/10.1149/2.023305jes	journal	January 2013
Characterization of Lithium Battery Materials During their Functioning in Using Dispersive XAS Ouvrard, G.; Bourgeon, N.; Guyomard, D. Physica Scripta https://doi.org/10.1238/Physica.Topical.115a00346	journal	January 2005
Xray Absorption Spectroscopy on Heterogeneous Catalysts at the new XAS Beamline at ANKA Grunwaldt, J. D.; Hannemann, S.; Gttlicher, J. Physica Scripta https://doi.org/10.1238/Physica.Topical.115a00769	journal	January 2005
Customization of an InHouse XAFS Spectrometer for Sulfur Measurement Taguchi, T.; Shinoda, K.; Tohji, K. Physica Scripta https://doi.org/10.1238/Physica.Topical.115a01017	journal	January 2005
Laboratory Dispersive EXAFS Spectrometer Mosset, A.; Lecante, P.; Baules, P. Acta Physica Polonica A, Vol. 91, Issue 4 https://doi.org/10.12693/APhysPolA.91.825	journal	April 1997
Generation of ultrashort hard-x-ray pulses with tabletop laser systems at a 2-kHz repetition rate Jiang, Yan; Lee, Taewoo; Rose-Petruck, Christoph G. Journal of the Optical Society of America B, Vol. 20, Issue 1 https://doi.org/10.1364/JOSAB.20.000229	journal	January 2003
Ultrafast laser-driven x-ray spectrometer for x-ray absorption spectroscopy of transition metal complexes Benesch, Frank; Lee, Taewoo; Jiang, Yan Optics Letters, Vol. 29, Issue 9 https://doi.org/10.1364/OL.29.001028	journal	January 2004
Laboratory Stopped-Flow XAFS Apparatus. Structure Determination of the Short-Lived Peroxochromium Intermediate Formed during Reduction Process of Chromate(VI) Ion by Hydrogen Peroxide Inada, Y.; Funahashi, S. Zeitschrift für Naturforschung B, Vol. 52, Issue 6 https://doi.org/10.1515/znb-1997-0608	journal	June 1997
Novel In Situ Probes for Nanocatalysis Stierle, Andreas; Molenbroek, Alfons M. MRS Bulletin, Vol. 32, Issue 12 https://doi.org/10.1557/mrs2007.208	journal	December 2007
Final Scientific Report: DE-SC0008580 Seidler, Gerald T. https://doi.org/10.2172/1347034	report	March 2017
X-ray Absorption Near Edge Structure Study on Valence Changes of Ni and Co in Li1-xNi0.82Co0.15M0.03O2 (M = Nb, Ti) Cathode Materials Hayakawa, Shinjiro; Kubouchi, Yuta; Hayashi, Tetsutaro Electrochemistry, Vol. 78, Issue 5 https://doi.org/10.5796/electrochemistry.78.454	journal	January 2010
Recent Improvements in Laboratory XAFS Facility Nishihagi, Kazuo; Kawabata, Atusi; Taniguchi, Kazuo Japanese Journal of Applied Physics, Vol. 32, Issue S2 https://doi.org/10.7567/JJAPS.32S2.258	journal	January 1993

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