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Effect of oxygen deficiency on the photoresponse and reactivity of mixed phase titania thin films

Journal Article · · Journal of Vacuum Science and Technology. A, International Journal Devoted to Vacuum, Surfaces, and Films
DOI:https://doi.org/10.1116/1.3574350· OSTI ID:22054030
; ; ;  [1]
  1. Department of Civil and Environmental Engineering, Northwestern University, 2145 Sheridan Road, Evanston, Illinois 60208 (United States)

Nonstoichiometric mixed phased titania nanocomposites (TiO{sub 2-x}) were deposited by reactive direct current magnetron sputtering. The authors explored the role of nonstoichiometry (as defined by oxygen deficiency in synthesis) in mixed phase titania thin films and its effects on the photoresponse and photocatalytic performance for CO{sub 2} reduction to methane under UV and visible light. Oxygen partial pressure was varied during film deposition, yielding different levels of oxygen deficiency in the films. Optimized nonstoichiometric films showed a strong redshift. The authors have identified an optimum set of synthesis conditions for TiO{sub 2-x} films that produce a relative maximum in photocatalytically produced methane under both UV and visible light.

OSTI ID:
22054030
Journal Information:
Journal of Vacuum Science and Technology. A, International Journal Devoted to Vacuum, Surfaces, and Films, Journal Name: Journal of Vacuum Science and Technology. A, International Journal Devoted to Vacuum, Surfaces, and Films Journal Issue: 3 Vol. 29; ISSN 1553-1813
Country of Publication:
United States
Language:
English

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