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Title: Combustion synthesis/densification of ceramics and ceramic composites. (Reannouncement with new availability information)

Technical Report ·
OSTI ID:200130

Combustion synthesis followed by densification was utilized in producing monolithic TiC and TiB2 materials, and TiC-Ni, TiB2-Ni, TiB2-Al2O3, and TiB2SiC ceramic composites. Static and dynamic densification equipments were developed with the loading applied immediately after the synthesis reaction was completed and the ceramic/composite was ductile. All the ceramics exhibited an equiaxed grain structure with alternating regions at high and low dislocation densities, indicating that recovery/recrystallization mechanisms are prevalent. The grain boundaries were, as far as could be established, devoid of impurities and second phases. Quasi-static and dynamic mechanical testing were performed and revealed that the materials exhibited strength levels comparable to conventionally produced materials. Instrumented densification experiments were conducted and a temperature-dependent consitutive model was applied for plastic deformation of the porous combustion synthesis product.

Research Organization:
California Univ., San Diego, CA (United States)
OSTI ID:
200130
Report Number(s):
AD-A-263811/2/XAB; CNN: Contract DAAL03-88-K-0194; TRN: 60510572
Resource Relation:
Other Information: PBD: 2 Sep 1992
Country of Publication:
United States
Language:
English