High pressure neutron diffraction on WAND2 with a Paris-Edinburgh press

Donnelly, Mary-Ellen; Wu, Yan; Kroll, Emily; Molaison, Jamie J.; Frontzek, Matthias D.; Haberl, Bianca

doi:10.1080/08957959.2022.2062242

High pressure neutron diffraction on WAND² with a Paris-Edinburgh press

Journal Article · Tue Apr 19 00:00:00 EDT 2022 · High Pressure Research

DOI:https://doi.org/10.1080/08957959.2022.2062242· OSTI ID:1879963

^[1]; ^[1]; Kroll, Emily ^[1]; ^[1]; ^[1]; ^[1]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

The Paris-Edinburgh press is a widely available, highly adaptable pressure cell commonly used while collecting neutron scattering data. Here, we detail the use of the VX3 and VX5 Paris-Edinburgh presses on the Wide-Angle Neutron Diffractometer (WAND²) at the High Flux Isotope Reactor at Oak Ridge National Laboratory. We first give a detailed overview of the instrument setup and alignment capabilities used at WAND². We then demonstrate the high pressure capabilities through three examples. In this work, the first example focuses on diffraction data obtained from a lithium-diamond mixture to 10 GPa with the use of single toroidal cubic boron nitride anvils. Other examples include the room temperature compressions of germanium (up to 16 GPa) and the mineral malachite with double toroidal sintered diamond anvils. This work thereby represents the first studies above 10 GPa at the High Flux Isotope Reactor and opens the door for future user experiments at these elevated pressures.

View Accepted Manuscript (DOE)

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States). High Flux Isotope Reactor (HFIR) and Spallation Neutron Source (SNS)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1879963

Journal Information:: High Pressure Research, Journal Name: High Pressure Research Journal Issue: 2 Vol. 42; ISSN 0895-7959

Publisher:: Taylor & FrancisCopyright Statement

Country of Publication:: United States

Language:: English

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72 PHYSICS OF ELEMENTARY PARTICLES AND FIELDS
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High pressure neutron diffraction on WAND2 with a Paris-Edinburgh press

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High pressure neutron diffraction on WAND² with a Paris-Edinburgh press