A Paris-Edinburgh Cell for High-Pressure and High-Temperature Structure Studies on Silicate Liquids Using Monochromatic Synchrotron Radiation

Yu, Tony; Prescher, Clemens; Ryu, Young Jay; Shi, Feng; Greenberg, Eran; Prakapenka, Vitali; Eng, Peter; Stubbs, Joanne; Kono, Yoshio; Shen, Guoyin; Watson, Heather; Rivers, Mark L.; Sutton, Stephen R.; Wang, Yanbin

doi:10.3390/min9110715

Title: A Paris-Edinburgh Cell for High-Pressure and High-Temperature Structure Studies on Silicate Liquids Using Monochromatic Synchrotron Radiation

Journal Article · Tue Nov 19 00:00:00 EST 2019 · Minerals

DOI:https://doi.org/10.3390/min9110715· OSTI ID:1635377

^[1]; Prescher, Clemens ^[1];

^[1]; Shi, Feng ^[1];

^[1]; Prakapenka, Vitali ^[1]; Eng, Peter ^[1]; Stubbs, Joanne ^[1]; Kono, Yoshio ^[2];

^[3]; Watson, Heather ^[4]; Rivers, Mark L. ^[1]; Sutton, Stephen R. ^[1]; Wang, Yanbin ^[1]

Univ. of Chicago, IL (United States)
Carnegie Inst. of Washington, Argonne, IL (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)
Union College, Schenectady, NY (United States)

A Paris-Edinburgh press combined with a multi-channel collimator assembly has been commissioned at the GeoSoilEnviro Center for Advanced Radiation Sources (GSECARS) beamline for monochromatic X-ray scattering, with an emphasis on studying low-Z liquids, especially silicate liquids at high pressure. The Paris-Edinburgh press is mounted on a general-purpose diffractometer, with a pixel array detector mounted on the detector arm. The incident monochromatic undulator beam with energies up to 60 keV is focused both horizontally and vertically to a beam size about 30 × 30 µm. With this setup, background scattering from the surrounding pressure media is completely removed at 2θ angles above 10° for samples larger than 1.05 mm in diameter. Thirty minutes is typically sufficient to collect robust X-ray scattering signals from a 1.6 mm diameter amorphous silicate sample. Cell assemblies for the standard Paris-Edinburgh anvils have been developed and pressures and temperatures up to 7 GPa and 2300 K, respectively, have been maintained steadily over hours. We have also developed a cupped-toroidal Drickamer anvil to further increase pressure and temperature capabilities. The cupped-toroidal Drickamer anvil combines features of a modified Drickamer anvil and the traditional Paris-Edinburgh anvil. Pressures up to 12 GPa have been generated at temperatures up to 2100 K.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: National Science Foundation (NSF); USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division; USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC02-06CH11357; FG02-94ER14466

OSTI ID:: 1635377

Journal Information:: Minerals, Vol. 9, Issue 11; ISSN 2075-163X

Publisher:: MDPICopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 5 works

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