Thermal stability of additively manufactured austenitic 304L ODS alloy

Ghayoor, Milad; Mirzababaei, Saereh; Sittiho, Anumat; Charit, Indrajit; Paul, Brian K.; Pasebani, Somayeh

doi:10.1016/j.jmst.2020.12.033

Thermal stability of additively manufactured austenitic 304L ODS alloy

Journal Article · Mon Jan 25 23:00:00 EST 2021 · Journal of Materials Science and Technology

DOI:https://doi.org/10.1016/j.jmst.2020.12.033· OSTI ID:1848624

Ghayoor, Milad ^[1]; Mirzababaei, Saereh ^[2]; Sittiho, Anumat ^[3]; Charit, Indrajit ^[3]; Paul, Brian K. ^[2]; Pasebani, Somayeh ^[2]

Oregon State Univ., Corvallis, OR (United States). School of Mechanical, Industrial and Manufacturing Engineering; Advanced Technology and Manufacturing Institute (ATAMI), Corvallis, OR (United States); Oregon State Univ., Corvallis, OR (United States)
Oregon State Univ., Corvallis, OR (United States). School of Mechanical, Industrial and Manufacturing Engineering; Advanced Technology and Manufacturing Institute (ATAMI), Corvallis, OR (United States)
Univ. of Idaho, Moscow, ID (United States). Materials Science and Engineering

Thermal stability and high-temperature mechanical properties of a 304L austenitic oxide dispersion strengthened (ODS) alloy manufactured via laser powder bed fusion (LPBF) are examined in this work. Additively manufactured 304L ODS alloy samples were aged at temperatures of 1000, 1100, and 1200 °C for 100 h in an argon atmosphere. Microstructure characterization of LPBF 304L ODS alloy before and after the thermal stability experiments revealed that despite the annihilation of dislocations, induced cellular substructure by the LPBF process was partially retained in the ODS alloy even after aging at 1200 °C. The size of Y-Si-O nanoparticles after aging at 1200 °C increased from 25 to 50 nm. EBSD analysis revealed that nanoparticles retained the microstructure of LPBF 304L ODS and hindered recrystallization and further grain growth. At 600 °C and 800 °C, the yield stress of the 290 and 145 MPa were measured, respectively, which are substantially higher than 113 MPa, and 68 MPa for 304L at the same temperatures. Furthermore, the creep properties of LPBF 304L ODS alloy were evaluated at a temperature of 700 °C under three applied stresses of 70, 85, and 100 MPa yielding a stress exponent (n) of ~7.7; the minimum creep rate at 100 MPa was found to be about two orders of magnitude lower than found in the literature for wrought 304L stainless steel.

View Accepted Manuscript (DOE)

Research Organization:: American Institute of Chemical Engineers (AIChE), New York, NY (United States)

Sponsoring Organization:: USDOE Office of Energy Efficiency and Renewable Energy (EERE); National Science Foundation (NSF)

Grant/Contract Number:: EE0007888

OSTI ID:: 1848624

Alternate ID(s):: OSTI ID: 1778580

Journal Information:: Journal of Materials Science and Technology, Journal Name: Journal of Materials Science and Technology Journal Issue: C Vol. 83; ISSN 1005-0302

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

References (48)

Fabrication of Fe-Cr-Al Oxide Dispersion Strengthened PM2000 Alloy Using Selective Laser Melting Walker, John C.; Berggreen, Kaj M.; Jones, Andy R. Advanced Engineering Materials, Vol. 11, Issue 7 https://doi.org/10.1002/adem.200800407	journal	July 2009
Additive Manufacturing of Ceramic-Based Materials: Additive Manufacturing of Ceramic-Based Materials Travitzky, Nahum; Bonet, Alexander; Dermeik, Benjamin Advanced Engineering Materials, Vol. 16, Issue 6 https://doi.org/10.1002/adem.201400097	journal	April 2014
The effect of oxide particle coherency on Zener pinning in ODS superalloys Mujahid, M.; Martin, J. W. Journal of Materials Science Letters, Vol. 13, Issue 3 https://doi.org/10.1007/BF00278146	journal	January 1994
The theory of Ostwald ripening Voorhees, P. W. Journal of Statistical Physics, Vol. 38, Issue 1-2 https://doi.org/10.1007/BF01017860	journal	January 1985
Fabrication of ODS Austenitic Steels and CoCrFeNi High-Entropy Alloys by Spark Plasma Sintering for Nuclear Energy Applications Yan, Xueliang; Zhang, Xiang; Wang, Fei JOM, Vol. 71, Issue 8 https://doi.org/10.1007/s11837-019-03531-7	journal	May 2019
Metal Powder Recyclability in Binder Jet Additive Manufacturing Mirzababaei, Saereh; Paul, Brian K.; Pasebani, Somayeh JOM, Vol. 72, Issue 9 https://doi.org/10.1007/s11837-020-04258-6	journal	July 2020
Additive Manufacturing of Ni-Rich NiTiHf20: Manufacturability, Composition, Density, and Transformation Behavior Nematollahi, M.; Toker, G.; Saghaian, S. E. Shape Memory and Superelasticity, Vol. 5, Issue 1 https://doi.org/10.1007/s40830-019-00214-9	journal	February 2019
The stability of the oxide dispersion in INCONEL alloy MA6000 Schaffer, G. B.; Loretto, M. H.; Smallman, R. E. Acta Metallurgica, Vol. 37, Issue 9 https://doi.org/10.1016/0001-6160(89)90053-9	journal	September 1989
Thermal stability of dispersoids in ferritic oxide-dispersion-strengthened alloys Krautwasser, P.; Czyrska-Filemonowicz, A.; Widera, M. Materials Science and Engineering: A, Vol. 177, Issue 1-2 https://doi.org/10.1016/0921-5093(94)90491-X	journal	April 1994
The relationship between transient and steady state creep in AISI 304 stainless steel Phaniraj, C.; Nandagopal, M.; Mannan, S. L. Acta Metallurgica et Materialia, Vol. 39, Issue 7 https://doi.org/10.1016/0956-7151(91)90253-W	journal	July 1991
Interfacial strained structure and orientation relationships of the nanosized oxide particles deduced from elasticity-driven morphology in oxide dispersion strengthened materials Ribis, J.; de Carlan, Y. Acta Materialia, Vol. 60, Issue 1 https://doi.org/10.1016/j.actamat.2011.09.042	journal	January 2012
Mechanical response and deformation mechanisms of ferritic oxide dispersion strengthened steel structures produced by selective laser melting Boegelein, Thomas; Dryepondt, Sebastien N.; Pandey, Amit Acta Materialia, Vol. 87 https://doi.org/10.1016/j.actamat.2014.12.047	journal	April 2015
Effects of atomizing media and post processing on mechanical properties of 17-4 PH stainless steel manufactured via selective laser melting Pasebani, Somayeh; Ghayoor, Milad; Badwe, Sunil Additive Manufacturing, Vol. 22 https://doi.org/10.1016/j.addma.2018.05.011	journal	August 2018
Oxide dispersion strengthened 304 L stainless steel produced by ink jetting and laser powder bed fusion Paul, Brian K.; Lee, Kijoon; He, Yujuan CIRP Annals, Vol. 69, Issue 1 https://doi.org/10.1016/j.cirp.2020.04.071	journal	January 2020
Enhancement of tensile properties due to microstructure optimization in ODS steels by zirconium addition Dong, Hongqing; Yu, Liming; Liu, Yongchang Fusion Engineering and Design, Vol. 125 https://doi.org/10.1016/j.fusengdes.2017.03.170	journal	December 2017
Temperature-induced buckling of ductile metals during cyclic loading and the subsequent early fracture Jirandehi, Arash P.; Mehdizadeh, M.; Khonsari, M. M. International Journal of Mechanical Sciences, Vol. 176 https://doi.org/10.1016/j.ijmecsci.2020.105525	journal	June 2020
Microstructure characterization and mechanical properties of laser additive manufactured oxide dispersion strengthened Fe-9Cr alloy Shi, Yingnan; Lu, Zheng; Xu, Haijian Journal of Alloys and Compounds, Vol. 791 https://doi.org/10.1016/j.jallcom.2019.03.284	journal	June 2019
Selective laser melting and tempering of H13 tool steel for rapid tooling applications Katancik, Michael; Mirzababaei, Saereh; Ghayoor, Milad Journal of Alloys and Compounds, Vol. 849 https://doi.org/10.1016/j.jallcom.2020.156319	journal	December 2020
Oxide dispersion-strengthened steels: A comparison of some commercial and experimental alloys Klueh, R. L.; Shingledecker, J. P.; Swindeman, R. W. Journal of Nuclear Materials, Vol. 341, Issue 2-3 https://doi.org/10.1016/j.jnucmat.2005.01.017	journal	May 2005
Correlation between chemical composition and size of very small oxide particles in the MA957 ODS ferritic alloy Sakasegawa, H.; Chaffron, L.; Legendre, F. Journal of Nuclear Materials, Vol. 384, Issue 2 https://doi.org/10.1016/j.jnucmat.2008.11.001	journal	February 2009
Fabrication and characterization of ODS austenitic steels Xu, Yingli; Zhou, Zhangjian; Li, Ming Journal of Nuclear Materials, Vol. 417, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2010.12.155	journal	October 2011
Processing and characterization of a hipped oxide dispersion strengthened austenitic steel Zhou, Zhangjian; Yang, Shuo; Chen, Wanhua Journal of Nuclear Materials, Vol. 428, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.08.027	journal	September 2012
Thermal stability of oxide particles in 12Cr ODS steel Mao, Xiaodong; Kim, Tae Kyu; Kim, Sung Soo Journal of Nuclear Materials, Vol. 428, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.09.011	journal	September 2012
Effects of plastic deformations on microstructure and mechanical properties of ODS-310 austenitic steel Wang, Man; Zhou, Zhangjian; Sun, Hongying Journal of Nuclear Materials, Vol. 430, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2012.07.014	journal	November 2012
Microstructure and mechanical behavior of ODS and non-ODS Fe–14Cr model alloys produced by spark plasma sintering Auger, M. A.; de Castro, V.; Leguey, T. Journal of Nuclear Materials, Vol. 436, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2013.01.331	journal	May 2013
Effects of milling process and alloying additions on oxide particle dispersion in austenitic stainless steel Oka, Hiroshi; Watanabe, Masashi; Ohnuki, Somei Journal of Nuclear Materials, Vol. 447, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.01.025	journal	April 2014
Development of low-Cr ODS FeCrAl alloys for accident-tolerant fuel cladding Dryepondt, Sebastien; Unocic, Kinga A.; Hoelzer, David T. Journal of Nuclear Materials, Vol. 501 https://doi.org/10.1016/j.jnucmat.2017.12.035	journal	April 2018
The interfacial orientation relationship of oxide nanoparticles in a hafnium-containing oxide dispersion-strengthened austenitic stainless steel Miao, Yinbin; Mo, Kun; Cui, Bai Materials Characterization, Vol. 101 https://doi.org/10.1016/j.matchar.2015.01.015	journal	March 2015
Long-term thermal-aging stability of a 16Cr-oxide dispersion strengthened ferritic steel at 973 K Li, S. F.; Zhou, Z. J.; Wang, P. H. Materials & Design, Vol. 90 https://doi.org/10.1016/j.matdes.2015.10.138	journal	January 2016
In-situ manufacturing of ODS FeCrAlY alloy via laser powder bed fusion Mirzababaei, Saereh; Ghayoor, Milad; Doyle, Ryan P. Materials Letters, Vol. 284 https://doi.org/10.1016/j.matlet.2020.129046	journal	February 2021
Mechanical properties and thermal stability of nanostructured ODS RAF steels Oksiuta, Z.; Lewandowska, M.; Kurzydłowski, K. J. Mechanics of Materials, Vol. 67 https://doi.org/10.1016/j.mechmat.2013.07.006	journal	December 2013
Microstructural observation and tensile properties of ODS-304 austenitic steel Wang, Man; Zhou, Zhangjian; Sun, Hongying Materials Science and Engineering: A, Vol. 559 https://doi.org/10.1016/j.msea.2012.08.099	journal	January 2013
Selective laser melting of an Al86Ni6Y4.5Co2La1.5 metallic glass: Processing, microstructure evolution and mechanical properties Li, X. P.; Kang, C. W.; Huang, H. Materials Science and Engineering: A, Vol. 606 https://doi.org/10.1016/j.msea.2014.03.097	journal	June 2014
On the remarkable thermal stability of nanostructured ferritic alloys Cunningham, N.; Wu, Y.; Klingensmith, D. Materials Science and Engineering: A, Vol. 613 https://doi.org/10.1016/j.msea.2014.06.097	journal	September 2014
Hardened austenite steel with columnar sub-grain structure formed by laser melting Saeidi, K.; Gao, X.; Zhong, Y. Materials Science and Engineering: A, Vol. 625 https://doi.org/10.1016/j.msea.2014.12.018	journal	February 2015
Oxide dispersion strengthened nickel based alloys via spark plasma sintering Pasebani, Somayeh; Dutt, Aniket K.; Burns, Jatuporn Materials Science and Engineering: A, Vol. 630 https://doi.org/10.1016/j.msea.2015.01.066	journal	April 2015
Selective laser melting of austenitic oxide dispersion strengthened steel: Processing, microstructural evolution and strengthening mechanisms Ghayoor, Milad; Lee, Kijoon; He, Yujuan Materials Science and Engineering: A, Vol. 788 https://doi.org/10.1016/j.msea.2020.139532	journal	June 2020
Tensile properties of mechanically alloyed Zr added austenitic stainless steel Morrall, Daniel; Gao, Jin; Zhang, Zhexian Nuclear Materials and Energy, Vol. 15 https://doi.org/10.1016/j.nme.2018.03.002	journal	May 2018
Microstructural Analysis of Additively Manufactured 304L Stainless Steel Oxide Dispersion Strengthened Alloy Ghayoor, Milad; Lee, Kijoon; He, Yujuan Microscopy and Microanalysis, Vol. 25, Issue S2 https://doi.org/10.1017/S1431927619013709	journal	August 2019
Additively manufactured hierarchical stainless steels with high strength and ductility Wang, Y. Morris; Voisin, Thomas; McKeown, Joseph T. Nature Materials, Vol. 17, Issue 1 https://doi.org/10.1038/nmat5021	journal	October 2017
An experimental investigation of extrapolation methods in the derivation of accurate unit-cell dimensions of crystals Nelson, J. B.; Riley, D. P. Proceedings of the Physical Society, Vol. 57, Issue 3 https://doi.org/10.1088/0959-5309/57/3/302	journal	May 1945
Recent Developments in Irradiation-Resistant Steels Odette, G. R.; Alinger, M. J.; Wirth, B. D. Annual Review of Materials Research, Vol. 38, Issue 1, p. 471-503 https://doi.org/10.1146/annurev.matsci.38.060407.130315	journal	August 2008
Austenitic Oxide Dispersion Strengthened Steels : A Review Raman, Lavanya; Gothandapani, Karthick; Murty, B. S. Defence Science Journal, Vol. 66, Issue 4 https://doi.org/10.14429/dsj.66.10205	journal	June 2016
Kinetics of sigma phase formation in a Duplex Stainless Steel Magnabosco, Rodrigo Materials Research, Vol. 12, Issue 3 https://doi.org/10.1590/S1516-14392009000300012	journal	September 2009
Additively Manufactured NiTi and NiTiHf Alloys: Estimating Service Life in High-Temperature Oxidation Dabbaghi, Hediyeh; Safaei, Keyvan; Nematollahi, Mohammadreza Materials, Vol. 13, Issue 9 https://doi.org/10.3390/ma13092104	journal	May 2020
Correlation between Milling Parameters, Structural and Mechanical Properties of Nanostructured Austenitic Y₂O₃ Strengthened Steels Koncz, Péter; Horváth, Ákos; Balázsi, Katalin Materials Science Forum, Vol. 729 https://doi.org/10.4028/www.scientific.net/MSF.729.409	journal	November 2012
Water Atomized 17-4 PH Stainless Steel Powder as a Cheaper Alternative Powder Feedstock for Selective Laser Melting Ghayoor, Milad; Badwe, Sunil B.; Irrinki, Harish Materials Science Forum, Vol. 941 https://doi.org/10.4028/www.scientific.net/MSF.941.698	journal	December 2018
Microstructural Observation and Tensile Isotropy of an Austenitic ods Steel Kim, Tae-Kyu; Bae, Chang-Soo; Kim, Do-Hyang Nuclear Engineering and Technology, Vol. 40, Issue 4 https://doi.org/10.5516/NET.2008.40.4.305	journal	June 2008

Similar Records

Laser Powder Bed Fusion Manufactured Alloys 625 and 282 and Properties Relevant to Advanced Nuclear Components

Technical Report · Mon Jun 30 20:00:00 EDT 2025 · OSTI ID:3002311

Selective laser melting of 304L stainless steel: Role of volumetric energy density on the microstructure, texture and mechanical properties

Journal Article · Thu Dec 26 23:00:00 EST 2019 · Additive Manufacturing · OSTI ID:1647744

Advanced ODS FeCrAl alloys for accident-tolerant fuel cladding

Technical Report · Mon Sep 01 00:00:00 EDT 2014 · OSTI ID:1150908

Related Subjects

36 MATERIALS SCIENCE
42 ENGINEERING
Aging
High-temperature
Laser powder bed fusion (LPBF)
Materials Science
Metallurgy & Metallurgical Engineering
Oxide dispersion strengthened (ODS) alloy
Thermal stability

Thermal stability of additively manufactured austenitic 304L ODS alloy

Citation Formats

References (48)

Similar Records

Related Subjects