Structural stability of mechanically alloyed amorphous (FeCoNi)70Ti10B20 under high-temperature and high-pressure

Avar, Baris; Simsek, Tuncay; Ozcan, Sadan; Chattopadhyay, Arun K.; Kalkan, Bora

doi:10.1016/j.jallcom.2020.158528

Title: Structural stability of mechanically alloyed amorphous (FeCoNi)₇₀Ti₁₀B₂₀ under high-temperature and high-pressure

Journal Article · Tue Dec 29 00:00:00 EST 2020 · Journal of Alloys and Compounds

DOI:https://doi.org/10.1016/j.jallcom.2020.158528· OSTI ID:1844934

Avar, Baris ^[1]; Simsek, Tuncay ^[2];

^[3]; Chattopadhyay, Arun K. ^[4]; Kalkan, Bora ^[5]

Zonguldak Bülent Ecevit Univ. (Turkey)
Kırıkkale Univ. (Turkey)
Hacettepe Univ., Ankara (Turkey)
Uniformity Labs, Fremont, CA (United States)
Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Univ. of California, Santa Cruz, CA (United States)

Nanostructured (FeCoNi)₇₀Ti₁₀B₂₀ (at%) alloy was synthesized by mechanical alloying from elemental powder mixture of Fe, Co, Ni, Ti and B using ball milling. The effect of ball milling time on the evolution of structure and morphology was investigated by X-ray diffraction, scanning and transmission electron microscopy and differential thermal analysis. It was observed that the formation of solid solution of (FeCoNi)₇₀Ti₁₀B₂₀ started from the very onset of the milling process. Crystallite size and lattice strains seemed to be leveled off after 20 h of milling with no further major changes. The milling process for longer periods introduced severe plastic deformations causing formation of amorphous phase of (FeCoNi)₇₀Ti₁₀B₂₀. The amorphous alloy composition was confirmed by energy dispersive X-ray spectroscopy analysis that showed an excellent homogeneity of the alloying elements. The phase stability of the mechanically alloyed amorphous sample was further verified by employing high-temperature and high-pressure studies. The alloy samples heat-treated at 700 °C revealed crystallization of the amorphous phase. However, synchrotron-based high-pressure ambient temperature X-ray diffraction studies confirmed that the amorphous phase of the alloy remained stable up to the pressure of 30 GPa. Here, the 50 h milled sample after being annealed at 350 °C showed improvement in the soft magnetic properties of the alloy, which was due to the probable elimination of the residual stress in the amorphous phase of the alloy powders.

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Research Organization:: Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC02-05CH11231

OSTI ID:: 1844934

Journal Information:: Journal of Alloys and Compounds, Vol. 860; ISSN 0925-8388

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

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36 MATERIALS SCIENCE
Mechanical alloying
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Title: Structural stability of mechanically alloyed amorphous (FeCoNi)70Ti10B20 under high-temperature and high-pressure

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Title: Structural stability of mechanically alloyed amorphous (FeCoNi)₇₀Ti₁₀B₂₀ under high-temperature and high-pressure