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Crystal growth and nucleation at metal-organic framework / solution interfaces

Technical Report ·
DOI:https://doi.org/10.2172/1840984· OSTI ID:1840984
 [1];  [2];  [2];  [2];  [2]
  1. Univ. of Wisconsin, Madison, WI (United States); University of Wisconsin - Madison
  2. Univ. of Wisconsin, Madison, WI (United States)

Metal-organic frameworks (MOFs) represent an incredibly diverse class of materials with equally diverse applications in catalysis, separations, and gas storage. Despite the prevalence of MOF structures in the literature, in many cases the synthesis of pure, crystalline MOF materials remains a significant challenge, with failed syntheses often yielding mixed crystalline or non-porous amorphous products. Our recent work aims to enable targeted MOF synthesis by developing a comprehensive and predictive model of the fundamental processes occurring at the MOF-solution interface under synthetically-relevant conditions. Our recent accomplishments include: (i) development and implementation of a graphics processor-accelerated approach to simulation the nucleation of weak electrolytes, and the extension of these methods to large/complex solutes such as MOFs; and (ii) studies of the structure of ZIF interfaces under conditions relevant to crystal growth; and (iii) addressing important open questions in the mechanism of MOF solvent-assisted linker exchange, and important synthetic pathway for MOFs.

Research Organization:
Univ. of Wisconsin, Madison, WI (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES). Chemical Sciences, Geosciences & Biosciences Division (CSGB)
DOE Contract Number:
SC0014059
OSTI ID:
1840984
Report Number(s):
DOE-UW--14059
Country of Publication:
United States
Language:
English

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