Large–Scale Syntheses of 2D Materials: Flash Joule Heating and Other Methods

Wyss, Kevin M.; Luong, Duy Xuan; Tour, James M.

doi:10.1002/adma.202106970

Large–Scale Syntheses of 2D Materials: Flash Joule Heating and Other Methods

Journal Article · Mon Oct 25 00:00:00 EDT 2021 · Advanced Materials

DOI:https://doi.org/10.1002/adma.202106970· OSTI ID:1881500

Wyss, Kevin M. ^[1]; Luong, Duy Xuan ^[2]; ^[2]

Rice Univ., Houston, TX (United States); Rice University
Rice Univ., Houston, TX (United States)

In the past 17 years, the larger-scale production of graphene and graphene family materials has proven difficult and costly, thus slowing wider-scale commercial applications. Here, the quality of the graphene that is prepared on larger scales has often been poor, demonstrating a need for improved quality controls. Here, current industrial graphene synthetic and analytical methods, as well as recent academic advancements in larger-scale or sustainable synthesis of graphene, defined here as weights more than 200 mg or films larger than 200 cm², are compiled and reviewed. There is a specific emphasis on recent research in the use of flash Joule heating as a rapid, efficient, and scalable method to produce graphene and other 2D nanomaterials. Reactor design, synthetic strategies, safety considerations, feedstock selection, Raman spectroscopy, and future outlooks for flash Joule heating syntheses are presented. To conclude, the remaining challenges and opportunities in the larger-scale synthesis of graphene and a perspective on the broader use of flash Joule heating for larger-scale 2D materials synthesis are discussed.

View Accepted Manuscript (DOE)

Research Organization:: Rice Univ., Houston, TX (United States)

Sponsoring Organization:: USDOE Office of Fossil Energy (FE), Clean Coal and Carbon Management

Grant/Contract Number:: FE0031794

OSTI ID:: 1881500

Alternate ID(s):: OSTI ID: 1839784

Journal Information:: Advanced Materials, Journal Name: Advanced Materials Journal Issue: 8 Vol. 34; ISSN 0935-9648

Publisher:: WileyCopyright Statement

Country of Publication:: United States

Language:: English

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