Lateral cracks during sliding indentation on various optical materials

Journal Article · Mon Sep 30 00:00:00 EDT 2019 · Journal of the American Ceramic Society

DOI:https://doi.org/10.1111/jace.16787· OSTI ID:1643777

Suratwala, Tayyab ^[1]; Steele, Rusty ^[1]; Shen, Nan ^[1]; Ray, Nathan ^[1]; Wong, Lana ^[1]; Miller, Phil E. ^[1]; Feit, Michael ^[1]

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1. Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

A series of static and sliding indentation (ie, scratching) was performed and characterized on a wide range of optical workpiece materials [single crystals of Al₂O₃ (sapphire), SiC, Y₃Al₅O₁₂ (YAG), CaF₂, and LiB₃O₅ (LBO); a SiO₂–Al₂O₃–P₂O₅–Li₂O glass ceramic (Zerodur); and glasses of SiO₂:TiO₂ (ULE), SiO₂ (fused silica), and P₂O₅–Al₂O₃–K₂O–BaO (Phosphate)] at various applied loads using various indenters (Vickers, 10 µm conical, and 200 µm conical). Despite having different load dependencies, the lateral crack depth formed during sliding indentation quantitatively scales with that formed during static indentation, explaining why static indentation has been historically effective in describing various grinding parameters. Depending on the indenter geometry, the amount of residual trench damage (plastic deformation and local fracturing) during sliding indentation was often enhanced by more than an order of magnitude compared with static indentation. A simple ploughing scratch model, which considers both tangential and normal stresses (where the tangential stress is amplified by relatively small tangential contact area), explains this enhancement and other observed trends. Accounting for the high correlation between residual trench depth and volumetric fracturing, the model is extended to estimate the amount of fracture damage as a function of the material properties of the workpiece, indenter geometry, and applied load. Such a model has utility in the design of optimized grinding processes, particularly the abrasive geometry. Finally, at higher loads (>1 N), lateral cracks were often observed to preferentially propagate in the forward scratching direction, as opposed to perpendicular to the scratch as typically observed. High-speed imaging of the scratch process confirms that these cracks propagate ahead of the sliding indenter during the scratching event. Finite element stress analysis suggests the ploughing frictional forces increase the mode I tensile stresses at the leading edge of the sliding indenter explaining the direction of crack propagation of such cracks.

• Research Organization: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
• Sponsoring Organization: USDOE National Nuclear Security Administration (NNSA)
• Grant/Contract Number: AC52-07NA27344
• OSTI ID: 1643777
• Alternate ID(s): OSTI ID: 1567889
• Report Number(s): LLNL--JRNL-781757; 976339
• Journal Information: Journal of the American Ceramic Society, Journal Name: Journal of the American Ceramic Society Journal Issue: 2 Vol. 103; ISSN 0002-7820
• Publisher: American Ceramic Society
• Country of Publication: United States
• Language: English

Related Subjects

36 MATERIALS SCIENCE
crack growth
fracture
fused silica
grinding
indentation
lasers
scratch