Emulation of fast reactor irradiated T91 using dual ion beam irradiation

Taller, Stephen; Jiao, Zhijie; Field, Kevin G.; Was, Gary S.

doi:10.1016/j.jnucmat.2019.151831

Title: Emulation of fast reactor irradiated T91 using dual ion beam irradiation

Journal Article · Wed Oct 02 00:00:00 EDT 2019 · Journal of Nuclear Materials

DOI:https://doi.org/10.1016/j.jnucmat.2019.151831· OSTI ID:1617812

Taller, Stephen ^[1]; Jiao, Zhijie ^[1];

^[2]; Was, Gary S. ^[1]

Univ. of Michigan, Ann Arbor, MI (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)

In this work, dual ion irradiations using 5 MeV defocused Fe²⁺ ions and co-injected He²⁺ ions were conducted on a ferritic-martensitic steel alloy, T91, in the temperature range of 406 °C–570 °C over a damage range of 14.6–35 dpa followed by characterization of the microstructure using transmission electron microscopy (TEM) and scanning transmission electron microscopy (STEM). Dislocation loops were observed to increase in diameter and decrease in density with temperature until only network dislocations were observed at the highest temperatures of 520 °C and 570 °C. Swelling exhibited the expected bell-shaped trend with temperature following the number density of cavities, peaking at 460 °C and with a bimodal size distribution except at 520 °C and 570 °C. Nickel- and silicon-rich clusters formed under dual ion irradiations near the surface at all but the highest temperatures of 520 °C and 570 °C. Very little Cr and Si segregation was observed at lath boundaries while Ni enriched at all temperatures examined. Segregation of Cr and Ni appeared to saturate by 17 dpa, while Si enriched up to 35 dpa. The dislocation and cavity microstructures of dual ion irradiated T91 and T91 irradiated in the BOR-60 fast reactor matched extremely well using a temperature shift of +60–70 °C. However, segregation to grain boundaries and formation of nickel-silicon rich clusters were minimal in the dual ion irradiated T91 and less than that in T91 irradiated in the BOR-60 fast reactor.

View Accepted Manuscript (DOE)

View Accepted Manuscript (Publisher)

Cite

Export

Save

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Nuclear Energy (NE); National Science Foundation (NSF)

Grant/Contract Number:: AC05-00OR22725; NE0000639; DMR-9871177; DMR-0320740

OSTI ID:: 1617812

Alternate ID(s):: OSTI ID: 1574525

Journal Information:: Journal of Nuclear Materials, Vol. 527, Issue C; ISSN 0022-3115

Publisher:: ElsevierCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 31 works

Citation information provided by
Web of Science

References (53)

Challenges to the use of ion irradiation for emulating reactor irradiation Was, Gary S. Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2015.73	journal	April 2015
Emulation of reactor irradiation damage using ion beams Was, G. S.; Jiao, Z.; Getto, E. Scripta Materialia, Vol. 88 https://doi.org/10.1016/j.scriptamat.2014.06.003	journal	October 2014
Effect of pre-implanted helium on void swelling evolution in self-ion irradiated HT9 Getto, E.; Jiao, Z.; Monterrosa, A. M. Journal of Nuclear Materials, Vol. 462 https://doi.org/10.1016/j.jnucmat.2015.01.045	journal	July 2015
Opportunities and limitations for ion beams in radiation effects studies: Bridging critical gaps between charged particle and neutron irradiations Zinkle, S. J.; Snead, L. L. Scripta Materialia, Vol. 143 https://doi.org/10.1016/j.scriptamat.2017.06.041	journal	January 2018
Helium effects on void formation in 9Cr-1MoVNb and 12Cr-1MoVW irradiated in HFIR Maziasz, P. J.; Klueh, R. L.; Vitek, J. M. Journal of Nuclear Materials, Vol. 141-143 https://doi.org/10.1016/0022-3115(86)90120-0	journal	November 1986
Microstructural evolution of HT9 under dual-beam charged particle irradiation Asano, K.; Kohno, Y.; Kohyama, A. Journal of Nuclear Materials, Vol. 155-157 https://doi.org/10.1016/0022-3115(88)90440-0	journal	July 1988
Microstructural evolution in dual-ion irradiated 316ss under various helium injection schedules Kohyama, Akira; Ayrault, Guy; Igata, Naohiro Journal of Nuclear Materials, Vol. 122, Issue 1-3 https://doi.org/10.1016/0022-3115(84)90600-7	journal	May 1984
The behavior of vacancy-type dislocation loops under electron irradiation in iron Wan, Farong; Zhan, Qian; Long, Yi Journal of Nuclear Materials, Vol. 455, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.05.048	journal	December 2014
Modification of radiation damage microstructure by helium Farrell, K.; Maziasz, P. J.; Lee, E. H. Radiation Effects, Vol. 78, Issue 1-4 https://doi.org/10.1080/00337578308207378	journal	January 1983
Effects of multi-beam irradiation on defect formation in Fe–Cr alloys Seto, H.; Hashimoto, N.; Kinoshita, H. Journal of Nuclear Materials, Vol. 417, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.01.053	journal	October 2011
The influence of helium on microstructuralevolution in an ion-irradiated low-swelling stainless steel Kenik, E. A. Journal of Nuclear Materials, Vol. 85-86 https://doi.org/10.1016/0022-3115(79)90335-0	journal	December 1979
High temperature radiation damage phenomena in complex alloys Rowcliffe, A. F.; Lee, Eal H. Journal of Nuclear Materials, Vol. 108-109 https://doi.org/10.1016/0022-3115(82)90500-1	journal	July 1982
Effects of pulsed and/or dual ion irradiation on microstructural evolution in a ti and si modified austenitic alloy Hishinuma, A.; Packan, N. H.; Lee, Eal H. Journal of Nuclear Materials, Vol. 122, Issue 1-3 https://doi.org/10.1016/0022-3115(84)90607-X	journal	May 1984
Effects of pulsed dual-ion irradiation on phase transformations and microstructure in Ti-modified austenitic alloy Lee, E. H.; Packan, N. H.; Mansur, L. K. Journal of Nuclear Materials, Vol. 117 https://doi.org/10.1016/0022-3115(83)90018-1	journal	July 1983
Helium effects in ion-bombarded 304 stainless steel Choyke, W. J.; Mcgruer, J. N.; Townsend, J. R. Journal of Nuclear Materials, Vol. 85-86 https://doi.org/10.1016/0022-3115(79)90333-7	journal	December 1979
Void swelling and microstructure evolution at very high damage level in self-ion irradiated ferritic-martensitic steels Getto, E.; Sun, K.; Monterrosa, A. M. Journal of Nuclear Materials, Vol. 480 https://doi.org/10.1016/j.jnucmat.2016.08.015	journal	November 2016
The influence of helium on cavity evolution in ion-irradiated T91 Monterrosa, Anthony M.; Jiao, Zhijie; Was, Gary S. Journal of Nuclear Materials, Vol. 509 https://doi.org/10.1016/j.jnucmat.2018.06.033	journal	October 2018
Simulation of first wall damage: Effects of the method of gas implantation Packan, N. H.; Farrell, K. Journal of Nuclear Materials, Vol. 85-86 https://doi.org/10.1016/0022-3115(79)90338-6	journal	December 1979
Mechanisms of helium interaction with radiation effects in metals and alloys: A review Mansur, L. K.; Coghlan, W. A. Journal of Nuclear Materials, Vol. 119, Issue 1 https://doi.org/10.1016/0022-3115(83)90047-8	journal	November 1983
Effect of irradiation mode on the microstructure of self-ion irradiated ferritic-martensitic alloys Getto, E.; Jiao, Z.; Monterrosa, A. M. Journal of Nuclear Materials, Vol. 465 https://doi.org/10.1016/j.jnucmat.2015.05.016	journal	October 2015
The influence of ion beam rastering on the swelling of self-ion irradiated pure iron at 450 °C Gigax, Jonathan G.; Aydogan, Eda; Chen, Tianyi Journal of Nuclear Materials, Vol. 465 https://doi.org/10.1016/j.jnucmat.2015.05.025	journal	October 2015
Comparison of swelling and irradiation creep behavior of fcc-austenitic and bcc-ferritic/martensitic alloys at high neutron exposure Garner, F. A.; Toloczko, M. B.; Sencer, B. H. Journal of Nuclear Materials, Vol. 276, Issue 1-3 https://doi.org/10.1016/S0022-3115(99)00225-1	journal	January 2000
TEM characterization of irradiated microstructure of Fe-9%Cr ODS and ferritic-martensitic alloys Swenson, M. J.; Wharry, J. P. Journal of Nuclear Materials, Vol. 502 https://doi.org/10.1016/j.jnucmat.2018.01.062	journal	April 2018
Microstructure evolution of T91 irradiated in the BOR60 fast reactor Jiao, Z.; Taller, S.; Field, K. Journal of Nuclear Materials, Vol. 504 https://doi.org/10.1016/j.jnucmat.2018.03.024	journal	June 2018
Resolution of the carbon contamination problem in ion irradiation experiments Was, G. S.; Taller, S.; Jiao, Z. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 412 https://doi.org/10.1016/j.nimb.2017.08.039	journal	December 2017
Multiple ion beam irradiation for the study of radiation damage in materials Taller, Stephen; Woodley, David; Getto, Elizabeth Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 412 https://doi.org/10.1016/j.nimb.2017.08.035	journal	December 2017
TEM characterization of dislocation loops in irradiated bcc Fe-based steels Yao, B.; Edwards, D. J.; Kurtz, R. J. Journal of Nuclear Materials, Vol. 434, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2012.12.002	journal	March 2013
Application of STEM characterization for investigating radiation effects in BCC Fe-based alloys Parish, Chad M.; Field, Kevin G.; Certain, Alicia G. Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2015.32	journal	April 2015
Multislice simulation of transmission electron microscopy imaging of helium bubbles in Fe Yao, B.; Edwards, D. J.; Kurtz, R. J. Journal of Electron Microscopy, Vol. 61, Issue 6 https://doi.org/10.1093/jmicro/dfs065	journal	October 2012
LAMDA: Irradiated-Materials Microscopy at Oak Ridge National Laboratory Parish, Chad M.; Kiran Kumar, N. A. P.; Snead, Lance L. Microscopy and Microanalysis, Vol. 21, Issue S3 https://doi.org/10.1017/S1431927615005814	journal	August 2015
The quantitative analysis of thin specimens Cliff, G.; Lorimer, G. W. Journal of Microscopy, Vol. 103, Issue 2 https://doi.org/10.1111/j.1365-2818.1975.tb03895.x	journal	March 1975
The morphology and crystallography of lath martensite in alloy steels Morito, S.; Huang, X.; Furuhara, T. Acta Materialia, Vol. 54, Issue 19 https://doi.org/10.1016/j.actamat.2006.07.009	journal	November 2006
Correlation of neutron and heavy-ion damage Mansur, L. K. Journal of Nuclear Materials, Vol. 78, Issue 1 https://doi.org/10.1016/0022-3115(78)90514-7	journal	November 1978
Theory of transitions in dose dependence of radiation effects in structural alloys Mansur, L. K. Journal of Nuclear Materials, Vol. 206, Issue 2-3 https://doi.org/10.1016/0022-3115(93)90130-Q	journal	November 1993
Microstructural evolution of proton irradiated T91 Gupta, G.; Jiao, Z.; Ham, A. N. Journal of Nuclear Materials, Vol. 351, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2006.02.028	journal	June 2006
Precipitate evolution in ion-irradiated HCM12A Jiao, Z.; Was, G. S. Journal of Nuclear Materials, Vol. 425, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.12.017	journal	June 2012
Radiation-induced swelling and radiation-induced segregation & precipitation in dual beam irradiated Ferritic/Martensitic HT9 steel Zheng, C.; Kaoumi, D. Materials Characterization, Vol. 134 https://doi.org/10.1016/j.matchar.2017.10.019	journal	December 2017
Phase stability in proton and heavy ion irradiated ferritic–martensitic alloys Jiao, Zhijie; Shankar, Vani; Was, Gary S. Journal of Nuclear Materials, Vol. 419, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2011.08.020	journal	December 2011
Radiation induced segregation and precipitation behavior in self-ion irradiated Ferritic/Martensitic HT9 steel Zheng, Ce; Auger, Maria A.; Moody, Michael P. Journal of Nuclear Materials, Vol. 491 https://doi.org/10.1016/j.jnucmat.2017.04.040	journal	August 2017
SANS and TEM of ferritic–martensitic steel T91 irradiated in FFTF up to 184dpa at 413°C Van den Bosch, J.; Anderoglu, O.; Dickerson, R. Journal of Nuclear Materials, Vol. 440, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2013.04.025	journal	September 2013
Microstructural stability of an HT-9 fuel assembly duct irradiated in FFTF Sencer, B. H.; Kennedy, J. R.; Cole, J. I. Journal of Nuclear Materials, Vol. 414, Issue 2 https://doi.org/10.1016/j.jnucmat.2011.03.050	journal	July 2011
G-phase precipitation in duplex stainless steels after long-term thermal aging: A high-resolution transmission electron microscopy study Li, Shilei; Wang, Yanli; Wang, Xitao Journal of Nuclear Materials, Vol. 452, Issue 1-3 https://doi.org/10.1016/j.jnucmat.2014.05.069	journal	September 2014
Effects of aging temperature on G-phase precipitation and ferrite-phase decomposition in duplex stainless steel Hamaoka, T.; Nomoto, A.; Nishida, K. Philosophical Magazine, Vol. 92, Issue 34 https://doi.org/10.1080/14786435.2012.707340	journal	December 2012
Characterization of microstructure and property evolution in advanced cladding and duct: Materials exposed to high dose and elevated temperature Allen, Todd R.; Kaoumi, Djamel; Wharry, Janelle P. Journal of Materials Research, Vol. 30, Issue 9 https://doi.org/10.1557/jmr.2015.99	journal	May 2015
The mechanism of radiation-induced segregation in ferritic–martensitic alloys Wharry, Janelle P.; Was, Gary S. Acta Materialia, Vol. 65 https://doi.org/10.1016/j.actamat.2013.09.049	journal	February 2014
Radiation-induced segregation in binary and ternary alloys Okamoto, P. R.; Rehn, L. E. Journal of Nuclear Materials, Vol. 83, Issue 1 https://doi.org/10.1016/0022-3115(79)90587-7	journal	August 1979
Irradiation-induced silicon segregation in ferritic steels Faulkner, R. G.; Song, S.; Flewitt, P. E. J. Journal of Nuclear Materials, Vol. 212-215 https://doi.org/10.1016/0022-3115(94)90132-5	journal	September 1994
The co-evolution of microstructure features in self-ion irradiated HT9 at very high damage levels Getto, E.; Vancoevering, G.; Was, G. S. Journal of Nuclear Materials, Vol. 484 https://doi.org/10.1016/j.jnucmat.2016.12.006	journal	February 2017
Primary damage formation in bcc iron Stoller, R. E.; Odette, G. R.; Wirth, B. D. Journal of Nuclear Materials, Vol. 251 https://doi.org/10.1016/S0022-3115(97)00256-0	journal	November 1997
Correlation of neutron and heavy-ion damage Packan, N. H.; Farrell, K.; Stiegler, J. O. Journal of Nuclear Materials, Vol. 78, Issue 1 https://doi.org/10.1016/0022-3115(78)90513-5	journal	November 1978
Nanocluster irradiation evolution in Fe-9%Cr ODS and ferritic-martensitic alloys Swenson, M. J.; Wharry, J. P. Journal of Nuclear Materials, Vol. 496 https://doi.org/10.1016/j.jnucmat.2017.08.045	journal	December 2017
Phase stability under irradiation: Ballistic effects Martin, G. Physical Review B, Vol. 30, Issue 3 https://doi.org/10.1103/PhysRevB.30.1424	journal	August 1984
Nucleation and growth of voids by radiation Mayer, R. M. Journal of Nuclear Materials, Vol. 95, Issue 1-2 https://doi.org/10.1016/0022-3115(80)90085-9	journal	November 1980

Similar Records

Solute segregation and precipitation across damage rates in dual-ion–irradiated T91 steel

Journal Article · Sat Feb 26 00:00:00 EST 2022 · Journal of Nuclear Materials · OSTI ID:1617812

Taller, Stephen A.; Pauly, Valentin; Jiao, Zhijie; +2 more

Microstructure evolution of T91 irradiated in the BOR60 fast reactor

Journal Article · Wed Mar 14 00:00:00 EDT 2018 · Journal of Nuclear Materials · OSTI ID:1617812

Jiao, Z.; Taller, S.; Field, K.; +3 more

The Role of Co-injected Helium on Swelling and Cavity Evolution at High Damage Levels in Ferritic-Martensitic Steels

Journal Article · Sun Feb 28 00:00:00 EST 2021 · Journal of Nuclear Materials · OSTI ID:1617812

Woodley, D.; Taller, S.; Jiao, Z.; +2 more

Related Subjects

36 MATERIALS SCIENCE
Microstructure
Swelling
Emulation
Ion irradiation
Ferritic-martensitic steel

Title: Emulation of fast reactor irradiated T91 using dual ion beam irradiation

Citation Formats

References (53)

Similar Records

Related Subjects